2024/10/01 更新

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写真a

ヤマサキ シゲト
山﨑 重人
YAMASAKI SHIGETO
所属
工学研究院 材料工学部門 准教授
工学部 材料工学科(併任)
工学府 材料工学専攻(併任)
職名
准教授
連絡先
メールアドレス
電話番号
0928022949
外部リンク

学位

  • 博士(工学)

研究テーマ・研究キーワード

  • 研究テーマ: 金属材料の高温変形

    研究キーワード: クリープ、ポルトヴァン-ルシャトリエ効果

    研究期間: 2007年4月

受賞

  • 研究奨励賞

    2021年3月   日本鉄鋼協会  

  • 日本鉄鋼協会 研究奨励賞

    2021年3月   日本鉄鋼協会  

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    日本鉄鋼協会より、鉄鋼及びその関連領域において優れた研究実績を挙げている若手研究・技術者に送られる賞

  • 俵論文賞

    2019年3月   日本鉄鋼協会  

  • 日本鉄鋼協会 俵論文賞

    2019年3月   日本鉄鋼協会  

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    研究論文(伊藤孝矩, 山﨑重人, 光原昌寿, 中島英治, 西田稔, 米村光治: 「金属間化合物により粒界被覆した多結晶Ni基耐熱合金の微細組織とクリープ特性」, 鉄と鋼, Vol.103, No.7, pp.434-442.)の内容が高く評価されたもの。

  • 金属組織写真賞 第2部門 奨励賞

    2016年3月   日本金属学会  

  • 日本金属学会 第66回金属組織写真賞, 奨励賞

    2016年3月   日本金属学会  

  • TOP 25 most downloaded articles for Scripta Materialia in the period April to June 2015

    2015年12月   Elsevier  

▼全件表示

論文

  • Relationship between Creep Strength and Magnetic Properties of Cobalt-bearing High Chromium Ferritic Steel 査読 国際誌

    Yamasaki, S., Mitsuhara, M. & Nakashima, H.

    isij international   2021年1月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • コバルト含有高クロムフェライト鋼のクリープ強度と磁気特性の関係 査読

    山﨑重人, 光原昌寿 & 中島英治,

    鉄と鋼   2020年11月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method 査読 国際誌

    Yamasaki, S., Deguchi, M., Mitsuhara, M., Nakashima, H., Ota, Y. & Kubushiro, K.

    Microscopy   2020年10月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • Kink Formation Process in Long-Period Stacking Ordered Mg-Zn-Y Alloy 査読 国際誌

    Shigeto Yamasaki, Tsubasa Tokuzumi Wansong Li, Masatoshi Mitsuhara, Koji Hagihara, Toshiyuki Fujii, Hideharu Nakashima

    Acta Materialia   195 ( 15 )   25 - 34   2020年8月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: https://doi.org/10.1016/j.actamat.2020.04.051

  • 窒素を有効利用した700℃級次世代耐熱フェライト鋼の開発

    山﨑重人、光原昌寿、中島英治

    ふぇらむ   24 ( 8 )   498 - 504   2019年8月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • Effect of Fe addition on heat-resistant aluminum alloys produced by selective laser melting 査読

    Shigeto Yamasaki, Tomo Okuhira, Masatoshi Mitsuhara, Hideharu Nakashima, Jun Kusui, Mitsuru Adachi

    Metals   9 ( 4 )   2019年4月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.3390/met9040468

  • Development of high-chromium ferritic heat-resistant steels with high nitrogen content 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    isij international   58 ( 6 )   1146 - 1154   2018年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2355/isijinternational.ISIJINT-2017-758

  • Deformation microstructure and fracture behavior in creep-exposed Alloy 617 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Materials Transactions   58 ( 3 )   442 - 449   2017年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/matertrans.M2016407

  • Development of high-chromium ferritic heat-resistant steels with high-nitrogen addition 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan   103 ( 1 )   64 - 72   2017年1月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2355/tetsutohagane.TETSU-2016-057

  • Evaluation of local creep strain in face-centred cubic heatresistant alloys using electron backscattered diffraction analysis 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima, Mitsuharu Yonemura

    isij international   57 ( 5 )   851 - 856   2017年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2355/isijinternational.ISIJINT-2016-712

  • 3D visualization of dislocation arrangement using scanning electron microscope serial sectioning method 査読

    S. Yamasaki, M. Mitsuhara, K. Ikeda, S. Hata, H. Nakashima

    Scripta Materialia   101   80 - 83   2015年5月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1016/j.scriptamat.2015.02.001

  • Low stress creep deformation in high chromium ferritic heat-resistant steel evaluated by helicoid spring creep test method 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Ken Ichi Ikeda, Satoshi Hata, Hideharu Nakashima

    Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan   100 ( 5 )   688 - 695   2014年5月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2355/tetsutohagane.100.688

  • Low-stress creep deformation in long-term aged ferritic heat-resistant steel 査読

    Shigeto Yamasaki, Masatoshi Mitsuhara, Ken Ichi Ikeda, Satoshi Hata, Hideharu Nakashima

    Materials Transactions   55 ( 5 )   842 - 849   2014年5月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/matertrans.M2013427

  • Strain Rate Dependence of Slip Persistence in TiZrNbHfTa Investigated with Microcantilever Bending Tests

    Tanaka M., Yamasaki S., Morikawa T.

    MATERIALS TRANSACTIONS   65 ( 9 )   1055 - 1060   2024年9月   ISSN:13459678 eISSN:13475320

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    記述言語:英語   出版者・発行元:公益社団法人 日本金属学会  

    The strain-rate dependence of slip persistence in TiZrNbHfTa was investigated using microcantilever bending tests instead of conventional single-crystal tensile tests. These tests were performed using micrometre-sized cantilevers fabricated within a grain of the polycrystalline material, and the ψ–χ relationship was obtained in detail. Bending tests were conducted in two strain rates to determine the ψ–χ relationship. The results showed that the slip plane macroscopically persisted on the {112} plane in the high-strain-rate test, while in the low-strain-rate test, the apparent slip plane roughly coincided with the plane where the maximum shear stress was applied. Detailed tracing of the slip bands, using atomic force microscopy, on the specimen surface showed that the slip plane was microscopically persisted on the {112} plane in high-strain-rate tests, while in low-strain-rate tests, the slip plane often cross-slipped between the {112} and {110} planes.

    DOI: 10.2320/matertrans.mt-ma2024010

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  • デジタル画像相関法と高分解能電子線後方散乱回折法の併用による微視・局所的な応力-ひずみ曲線情報のマッピング

    山﨑 重人, 松尾 啓史, 森川 龍哉, 田中 將己

    日本金属学会誌   88 ( 9 )   216 - 225   2024年9月   ISSN:00214876 eISSN:18806880

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    記述言語:日本語   出版者・発行元:公益社団法人 日本金属学会  

    Microscopic stress–strain curves were obtained by applying stress measurements using the HR–EBSD method and strain measurements using the DIC method to the same field of view in SEM in–situ tensile tests. From the analysis of these microscopic stress–strain curves, yield stress map and work hardening rate map were successfully produced. The relationship between these mechanical property value maps and the microstructure is investigated. The yield stress maps confirm the tendency of the local yield stress to show different values for different grains, but the Schmid factor alone cannot explain the magnitude of the yield stress. When adjacent grains with significantly different Schmid factors deformed cooperatively, the yield stress is found to increase as a result of stress partitioning. Localized regions of extreme work hardening rates were observed in the work hardening rate maps. These regions were located close to grain boundaries with low mA values where slip transfer was difficult and an interruption of the slip bands was observed. In addition, the rate of increase of GND density with strain was large in these regions. From these results, it can be understood that the extreme work hardening rates are due to increased back stresses caused by the accumulation of dislocations on low mA grain boundaries.

    DOI: 10.2320/jinstmet.j202404

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  • Plastic anisotropy in yield stress of drawn pearlitic steels

    Akada, T; Ueji, R; Mitsuhara, M; Yamasaki, S; Tanaka, M

    MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING   898   2024年4月   ISSN:0921-5093 eISSN:1873-4936

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    掲載種別:研究論文(学術雑誌)   出版者・発行元:Materials Science and Engineering: A  

    Plastic anisotropy in the yield stress of pearlitic steels evolved by drawing was studied. The tension and compression tests were performed in parallel and perpendicular directions to the drawing direction. The yield stress in the parallel tension and vertical compression tests increased with the increase in drawing strain. On the other hand, in the parallel compression, the yield stress decreased significantly at the small drawing strain and then increased at the larger strain. The difference between the yield stress at the tension and at the compression did not change largely after the start of the drawing. The observation of microstructure indicated no significant heterogeneity of the deformation microstructure and texture at the different locations in the radial direction of the drawn samples, meaning that the plastic anisotropy was brought by reasons other than the non-uniformity of the deformation condition. The measurement of the distribution of the local misorientation in ferrite suggested the large plastic deformation even at smaller strain by drawing. This result indicates that the residual stress in plastically deformed ferrite brings back stress, which can be the source of the plastic anisotropy.

    DOI: 10.1016/j.msea.2024.146380

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  • Thermoelectric Properties of Ba<sub>8</sub>Cu<i><sub>x</sub></i>Si<i><sub>y</sub></i>Ge<sub>46-<i>x</i>-<i>y</i> </sub> Clathrates Synthesized by the Czochralski Method

    Takagi, K; Matsukawa, Y; Araki, S; Saeki, R; Yamasaki, S; Arita, M; Munetoh, S

    ACS APPLIED ENERGY MATERIALS   7 ( 7 )   2665 - 2670   2024年3月   ISSN:2574-0962

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    出版者・発行元:ACS Applied Energy Materials  

    A type-I clathrate Ba8CuxSiyGe46-x-y ingot consisting of millimeter-sized grains with different crystallographic orientations was synthesized by the Czochralski method. The lower part of the ingot contained more Cu and Ge within the clathrate phase. The electrical resistivities of the top, middle, and bottom of the ingot at 550 °C were 0.78, 1.72, and 1.55 mΩ·cm, respectively. The differences in these values are consistent with the carrier concentration and calculated anisotropic effective mass of the electrons, which are based on the actual chemical composition and crystal orientation, respectively. The resistivity of the top part with few grain boundaries is less than a quarter of that of the hot-pressed sample with a similar composition. Despite the different carrier concentrations, the Seebeck coefficient of all parts had similar values of approximately −120 μV/K at 550 °C. The thermal conductivity at 350 °C was approximately 3.0 W/m·K for top part and 2.5 W/m·K for middle and bottom parts, about 1.5-1.8 times larger than those of previous reported hot-pressed samples. The power factor and dimensionless figure of merit ZT value of the top reached 18.8 μW/cm·K2 and 0.34, respectively. These results indicate that fabrication by the Czochralski method can improve the thermoelectric performance of Ba8CuxSiyGe46-x-y clathrates.

    DOI: 10.1021/acsaem.3c02961

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  • 局所的なひずみの不均一分布とマクロな応力-ひずみ曲線を同時に再現する試み

    髙橋 学, 上野 虎太郎, 坂口 健太, 林 宏太郎, 川田 裕之, 山﨑 重人

    鉄と鋼   110 ( 3 )   90 - 100   2024年2月   ISSN:00211575 eISSN:18832954

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    記述言語:日本語   出版者・発行元:一般社団法人 日本鉄鋼協会  

    A modified continuum composite model was utilized to analyze the stress–strain behavior of asquenched steels with a fully martensitic microstructure. The model was employed to express the stress– strain curves obtained by a simple tensile test and those obtained by forward and backward loading using a simple shear test machine. The study confirmed that the model can represent the stress–strain behavior under both forward and backward deformation. In addition, the evolution of local strain distributions during plastic deformation was investigated using a digital image correlation method. The strain distributions and their evolution during deformation were qualitatively represented using this model. The discrepancies between the model calculations and experiments are due to the limitations of the iso-work assumption and the impact of slip deformation on the macroscopic work-hardening behavior of martensitic steels. Highly strain-concentrated regions aligned along the longitudinal direction of the lath and block, known as in-lath-plane slips, may not play an important role in the work-hardening behavior of as-quenched martensitic steels. However, the other slips, namely the out-of-lath slip, may play a significant role in the work hardening of as-quenched martensitic steels.

    DOI: 10.2355/tetsutohagane.tetsu-2023-063

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  • Bridging between Heterogeneous Local Strain Distribution and Macroscopic Stress- strain Curves

    Takahashi, M; Ueno, K; Sakaguchi, K; Hayashi, K; Kawata, H; Yamasaki, S

    ISIJ International   64 ( 2 )   345 - 353   2024年1月   ISSN:09151559 eISSN:13475460

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    記述言語:英語   出版者・発行元:一般社団法人 日本鉄鋼協会  

    A modified continuum composite model was utilized to analyze the stress-strain behavior of as-quenched steels with a fully martensitic microstructure. The model was employed to express the stress-strain curves obtained by a simple tensile test and those obtained by forward and backward loading using a simple shear test machine. The study confirmed that the model can represent the stress-strain behavior under both forward and backward deformation. In addition, the evolution of local strain distributions during plastic deformation was investigated using a digital image correlation method. The strain distributions and their evolution during deformation were qualitatively represented using this model. The discrepancies between the model calculations and experiments are due to the limitations of the iso-work assumption and the impact of slip deformation on the macroscopic work-hardening behavior of martensitic steels. Highly strain-concentrated regions aligned along the longitudinal direction of the lath and block, known as in-lath-plane slips, may not play an important role in the work-hardening behavior of as-quenched martensitic steels. However, the other slips, namely the out-of-lath slip, may play a significant role in the work hardening of as-quenched martensitic steels.

    DOI: 10.2355/isijinternational.isijint-2023-140

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  • FIB-SEMによる転位組織の三次元観察

    山﨑 重人

    顕微鏡   58 ( 3 )   90 - 94   2023年12月   ISSN:13490958 eISSN:24342386

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    記述言語:日本語   出版者・発行元:公益社団法人 日本顕微鏡学会  

    <p>クリープ変形させたニッケル基耐熱合金に対して,SEM-ECCI像のシリアルセクショニングによる転位の三次元可視化を行った.ECCI像の連続断層像を基に計算を行うことで,転位組織を含む約5 μm × 5 μm × 0.3 μmのボリュームの再構築に成功した.これに,SEM-EBSD法によって得られた結晶方位情報を組み込むことによって,すべり面や交差すべりなどの転位の三次元的な配置が三次元ボリュームに正確に反映されていることを確認した.このように,ECCI像のシリアルセクショニングによって,バルクの転位組織をマイクロメートルスケールの範囲で三次元的に観察・解析することが可能である.</p>

    DOI: 10.11410/kenbikyo.58.3_90

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  • <i>β</i>型チタン合金Ti-22V-4Alにおける変形・破壊挙動の温度依存性

    矢野 伶, 田中 將己, 山﨑 重人, 森川 龍哉, 都留 智仁

    軽金属   73 ( 10 )   497 - 503   2023年10月   ISSN:04515994 eISSN:18808018

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)   出版者・発行元:一般社団法人 軽金属学会  

    Impact tests and tensile tests were conducted between 77 K and 450 K in order to elucidate the temperature dependence of absorbed-impact energy, yield stress, effective shear stress, activation volume, and activation enthalpy. The impact-absorbed energy decreased with decreasing test temperature, however, this alloy did not undergo low-temperature embrittlement although it has a bcc structure. Tensile tests showed changes in both the work-hardening rate and the temperature dependence of yield stress at approximately 150 K. This suggests a change in the mechanism behind the plastic deformation at the temperature. The temperature dependence of the activation enthalpy for dislocation glide suggests that the process of climbing over the Peierls potential (kink-pair nucleation) is the dominant mechanism for the dislocation glide from 150 K to 200 K, while the interaction between a dislocation and solute atoms dominantly controls the dislocation glide above 200 K. Superelasticity appears in stress-strain curves tested below 120 K, suggesting that the yielding is governed by transformation-induced plasticity below 120 K. The enhanced toughness at low temperatures in these alloys is discussed from the viewpoint of dislocation shielding theory.

    DOI: 10.2464/jilm.73.497

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  • Acquisition of microscopic and local stress-strain curves by combination of HR-EBSD and DIC methods

    Yamasaki, S; Matsuo, H; Morikawa, T; Tanaka, M

    SCRIPTA MATERIALIA   235   115603 - 115603   2023年10月   ISSN:1359-6462 eISSN:1872-8456

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    記述言語:その他   掲載種別:研究論文(学術雑誌)   出版者・発行元:Scripta Materialia  

    A method for obtaining microscopic and localized stress-strain curves is proposed by combining strain measurements using the digital image correlation (DIC) method with stress measurements using high-resolution electron backscattered diffraction (HR-EBSD). A dataset containing 11 steps of stress–strain information in a single subset was created by applying georeferencing to DIC strain maps and HR-EBSD stress maps measured in a deformation-interrupted microstructure. This analysis allowed us to obtain local stress-strain curves and strain energy maps of polycrystalline nickel alloys. A comparison of the stress-strain curves obtained from any subset in the map revealed that these curves show extremely diverse shapes depending on the location in the microstructure.

    DOI: 10.1016/j.scriptamat.2023.115603

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  • Micromechanical testing for quantitative characterization of apparent slip system: Extinction of persistence of slip in carbon bearing Fe-3% Si

    田中 將己, タネナカ マサノリ, 山﨑 重人, 森川 龍哉

    Scripta Materialia   232   115473   2023年7月   ISSN:13596462

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    記述言語:英語   出版者・発行元:Elsevier  

    The effect of carbon on the persistence of the slip in Fe–3 mass% Si was investigated. We applied micro-sized cantilever bending tests to obtain ψ–χ relationships that enable quantitative analysis of the persistence of the slip. It was demonstrated that the result from decarburized specimens using this method is consistent with those obtained in previous studies from bulk-sized tensile test specimens. This novel method eliminates the difficulty of preparing bulk-sized single-crystal specimens for investigating the persistence of the slip. The persistence of the slip weakened in aged specimens containing 0.016 mass% C and disappeared in quenched specimens with the same carbon content, where wavy slip bands were observed. The reason for these changes in the macroscopically apparent slip plane is explained by the assumption that the frequency of nucleating kink-pair in the competitive {110} planes is a function of the resolved shear stress.

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  • Micromechanical testing for quantitative characterization of apparent slip system: Extinction of persistence of slip in carbon bearing Fe-3% Si

    Tanaka, M; Takenaka, M; Yamasaki, S; Morikawa, T

    SCRIPTA MATERIALIA   232   2023年7月   ISSN:1359-6462 eISSN:1872-8456

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    掲載種別:研究論文(学術雑誌)   出版者・発行元:Scripta Materialia  

    The effect of carbon on the persistence of the slip in Fe–3 mass% Si was investigated. We applied micro-sized cantilever bending tests to obtain ψ–χ relationships that enable quantitative analysis of the persistence of the slip. It was demonstrated that the result from decarburized specimens using this method is consistent with those obtained in previous studies from bulk-sized tensile test specimens. This novel method eliminates the difficulty of preparing bulk-sized single-crystal specimens for investigating the persistence of the slip. The persistence of the slip weakened in aged specimens containing 0.016 mass% C and disappeared in quenched specimens with the same carbon content, where wavy slip bands were observed. The reason for these changes in the macroscopically apparent slip plane is explained by the assumption that the frequency of nucleating kink-pair in the competitive {110} planes is a function of the resolved shear stress.

    DOI: 10.1016/j.scriptamat.2023.115473

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  • Temperature dependence of the yield stress in TiZrNbHfTa body-centred cubic high-entropy alloy

    田中 將己, 山﨑 重人, 森川 龍哉

    Materials Science and Engineering A   871   144917   2023年4月   ISSN:09215093 eISSN:18734936

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    記述言語:英語   出版者・発行元:Elsevier  

    Body-centred cubic (bcc) high-entropy alloys exhibit high strength. However, their yield behaviour and controlling mechanisms are still ambiguous. In this study, the temperature dependence of the yield stress, effective stress, activation volume, and activation enthalpy in a polycrystalline bcc refractory high-entropy alloy of TiZrNbHfTa were measured by tensile tests at 77–750 K. At temperatures above 650 K, the temperature dependence of the yield stress disappeared, and serration appeared in stress–strain curves. By extrapolating the effective shear stress to 0 K, the Peierls stress was estimated to be 580 MPa. The value was compared with different crystals using the relationship (τ_p)/(μ) and (h)/(b) , where τ_p is the Peierls stress, μ is the shear modulus, h is the distance between the slip planes, and b is the Burgers vector. The (τ_p)/(μ) value in this study was slightly higher than that of other bcc crystals. The activation enthalpy below 260 K corresponds to that of other bcc crystals with high Peierls potentials, suggesting kink-pair nucleation is the controlling mechanism of the dislocation glide in this temperature range. Meanwhile, the activation enthalpy above 260 K deviated from the trendline, indicating the changes in the dislocation glide from the kink-pair nucleation to other one.

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  • Temperature dependence of the yield stress in TiZrNbHfTa body-centred cubic high-entropy alloy

    Tanaka, M; Yamasaki, S; Morikawa, T

    MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING   871   2023年4月   ISSN:0921-5093 eISSN:1873-4936

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    掲載種別:研究論文(学術雑誌)   出版者・発行元:Materials Science and Engineering: A  

    Body-centred cubic (bcc) high-entropy alloys exhibit high strength. However, their yield behaviour and controlling mechanisms are still ambiguous. In this study, the temperature dependence of the yield stress, effective stress, activation volume, and activation enthalpy in a polycrystalline bcc refractory high-entropy alloy of TiZrNbHfTa were measured by tensile tests at 77–750 K. At temperatures above 650 K, the temperature dependence of the yield stress disappeared, and serration appeared in stress–strain curves. By extrapolating the effective shear stress to 0 K, the Peierls stress was estimated to be 580 MPa. The value was compared with different crystals using the relationship [Formula presented] and [Formula presented], where τp is the Peierls stress, μ is the shear modulus, h is the distance between the slip planes, and b is the Burgers vector. The [Formula presented] value in this study was slightly higher than that of other bcc crystals. The activation enthalpy below 260 K corresponds to that of other bcc crystals with high Peierls potentials, suggesting kink-pair nucleation is the controlling mechanism of the dislocation glide in this temperature range. Meanwhile, the activation enthalpy above 260 K deviated from the trendline, indicating the changes in the dislocation glide from the kink-pair nucleation to other one.

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  • Role of disclinations around kink bands on deformation behavior in Mg-Zn-Y alloys with a long-period stacking ordered phase

    Tokuzumi, T; Mitsuhara, M; Yamasaki, S; Inamura, T; Fujii, T; Nakashima, H

    ACTA MATERIALIA   248   2023年4月   ISSN:1359-6454 eISSN:1873-2453

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    掲載種別:研究論文(学術雑誌)   出版者・発行元:Acta Materialia  

    Mg–Zn–Y alloys that contain an Mg-based long-period stacking ordered (LPSO) phase exhibit excellent mechanical properties because of the kink bands formed by plastic deformation. Such “kink-band strengthening” has attracted significant attention. Herein, we conducted deformation tests on directionally solidified single-phase LPSO Mg85Zn6Y9 alloys to investigate the kink-band strengthening mechanism. High-angular resolution electron backscatter diffraction was performed to detect misorientation between the matrices on either side of the kink bands. The misorientations corresponded to the magnitudes of the Frank vectors of the disclinations around the kink, and closely matched the estimations from geometric analysis, which supported the existence of disclinations. Moreover, the Frank vector of the kink bands increased after shear deformation, which indicates that shear deformation introduced new disclinations around the kinks. Scanning electron microscopy demonstrated that the kinks clearly obstructed basal ⟨a⟩ slip. Furthermore, scanning transmission electron microscopy of a sheared kink band revealed dislocation pile-ups on both sides of the kink/matrix interface, as well as the formation of secondary kinks that stabilized the structure against shear deformation (i.e., self-accommodation) and bend contours caused by elastic stress fields. The results suggest that disclinations behave as long-range obstacles to dislocation motion (e.g., by reducing the increase in kink-band self-energy or by the elastic stress field of disclinations). We believe that this study will play a key role in identifying the factors responsible for kink-band strengthening in LPSO-phase Mg alloys and in understanding the phenomena underlying the strengthening mechanism.

    DOI: 10.1016/j.actamat.2023.118785

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  • Tensile Deformation Behaviors of Pure Ti with Different Grain Sizes under Wide-Range of Strain Rate

    Deguchi, M; Yamasaki, S; Mitsuhara, M; Nakashima, H; Tsukamoto, G; Kunieda, T

    MATERIALS   16 ( 2 )   2023年1月   ISSN:1996-1944 eISSN:1996-1944

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    記述言語:英語   掲載種別:研究論文(学術雑誌)   出版者・発行元:Materials  

    In this study, pure titanium equivalent to Grade 1 was subjected to tensile tests at strain rates ranging from 10−6 to 100 s−1 to investigate the relationship between its mechanical properties and its twinning and slip. Deformation properties and microstructures of samples having average grain sizes of 210 μm (Ti-210), 30 μm (Ti-30), and 5 μm (Ti-5) were evaluated. With increasing strain rates, the 0.2% proof stress and ultimate tensile strength increased for all samples; the fracture strain increased for Ti-210, decreased for Ti-5, and changed negligibly for Ti-30. Comparing high (100 s−1) and low (10−6 s−1) strain rates, twinning occurred more frequently in Ti-30 and Ti-210 at high strain rates, but the frequency did not change in Ti-5. The frequency of 1st order pyramidal slip tended to be higher in Ti-30 and Ti-5 at low strain rates. The higher ductility exhibited by Ti-210 at high strain rates was attributed to the high frequency of twinning. In contrast, the higher ductility of Ti-5 at low strain rates was attributed to the activity of the 1st order pyramidal slip.

    DOI: 10.3390/ma16020529

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  • Microstructural Size Effect on Strain-Hardening of As-quenched Low Alloyed Martensitic Steels

    Takahashi M., Sakaguchi K., Kawata H., Hayashi K., Yamasaki S.

    28th IFHTSE 2023 Congress   2023年   ISBN:9781713889533

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    出版者・発行元:28th IFHTSE 2023 Congress  

    Quenched martensitic steels are known to show the characteristic feature of stress-strain relations, with extremely low elastic limits and very large work-hardening. The continuum composite approach is one way to express this characteristic feature of stress-strain curves. Although the overall stress-strain curves, as a function of alloy chemistries of steels, were well represented by this approach, the relationship between the macroscopic deformation behaviors and microstructural information is yet to be clarified. A high-spatial-resolution digital image correlation analysis was conducted to demonstrate the possible unit size corresponding to the microstructure. The continuum composite approach model was also modified to consider the size effect of the microstructure on the stress-strain curves of the as-quenched martensitic steels. Strain concentrations were observed at various boundaries, including lath boundaries, and the characteristic microstructural size was also predicted by the present model, which is smaller than the reported spacing between adjacent strain-concentrated regions.

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  • 窒素または炭素を含有するLaves強化型フェライト系耐熱鋼のクリープ変形挙動と微細組織

    山﨑 重人, 光原 昌寿, 中島 英治, 木村 一弘

    鉄と鋼   109 ( 3 )   167 - 178   2023年   ISSN:00211575 eISSN:18832954

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)   出版者・発行元:一般社団法人 日本鉄鋼協会  

    The creep deformation behavior and microstructure of a N-containing steel expected to exhibit high creep strength and excellent oxidation resistance were investigated. Even for steel with a high W content, it was possible to form a martensitic microstructure by adding a sufficient amount of N. Comparison of the microstructures of the N-containing steel and a C-containing steel confirmed that the two steels have the same crystal orientation relationship. The N-containing steel precipitated with the Laves phase as a strengthening phase displayed a higher creep strength than conventional steel under relatively high stress. However, the superiority of the creep strength of the N-containing steel relative to the conventional steel decreased under low stress. The stress exponent of the N-containing steel was different from those of the C-containing steel and the conventional steel. This deference considered to be ascribed to the difference of variation behavior of dislocation density during creep deformation.

    DOI: 10.2355/tetsutohagane.tetsu-2022-065

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  • Microstructural Size Effect on Strain-Hardening of As-Quenched Low-Alloyed Martensitic Steels

    Sakaguchi, K; Yamasaki, S; Kawata, H; Hayashi, K; Takahashi, M

    ISIJ International   62 ( 10 )   2008 - 2015   2022年10月   ISSN:09151559 eISSN:13475460

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    記述言語:英語   出版者・発行元:一般社団法人 日本鉄鋼協会  

    Quenched martensitic steels are known to show the characteristic feature of stress–strain relations, with extremely low elastic limits and very large work-hardening. The continuum composite approach is one way to express this characteristic feature of stress–strain curves. Although the overall stress–strain curves, as a function of alloy chemistries of steels, were well represented by this approach, the relationship between the macroscopic deformation behaviors and microstructural information is yet to be clarified. A high-spatial-resolution digital image correlation analysis was conducted to demonstrate the possible unit size corresponding to the microstructure. The continuum composite approach model was also modified to consider the size effect of the microstructure on the stress–strain curves of the as-quenched martensitic steels. Strain concentrations were observed at various boundaries, including lath boundaries, and the characteristic microstructural size was also predicted by the present model, which is smaller than the reported spacing between adjacent strain-concentrated regions.

    DOI: 10.2355/isijinternational.isijint-2022-114

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  • Sulfide Stress Cracking (SSC) of Low Alloy Linepipe Steels in Low H2S Content Sour Environment

    Shimamura, J; Morikawa, T; Yamasaki, S; Tanaka, M

    ISIJ International   62 ( 10 )   2095 - 2106   2022年10月   ISSN:09151559 eISSN:13475460

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    記述言語:その他   掲載種別:研究論文(学術雑誌)   出版者・発行元:一般社団法人 日本鉄鋼協会  

    Resistance to Sulfide Stress Cracking (SSC) caused by local hard zones of pipe inner surface has been required in low alloy linepipe steel. In this study, using two samples with different surface hardness, the detailed SSC initiation behavior was clarified by four-point bend (4PB) SSC tests in which immersion time and applied stress were changed in a sour environment containing 0.15 bar hydrogen sulfide (H2S) gas. SSC cracks occurred when the applied stress was higher than 90% actual yield strength (AYS) in higher surface hardness samples over 270 HV0.1. From the fracture surface observation of SSC crack sample, it was found that the mechanism gradually shifted from active path corrosion (APC) to hydrogen embrittlement (HE), and that the influence of APC mechanism remained partially in the process of SSC initiation at the tip of corrosion pit or groove. The polarization measurement in the 4PB SSC test showed that the anodic and cathodic reactions (especially cathodic reactions) were activated when the applied stress was 90% AYS or higher. The FEM coupled analysis simulating the stress and strain concentration at the bottom tip of the corrosion groove and the hydrogen diffusion and accumulation was carried out. The principal stress in the tensile direction showed the maximum value at 0.04–0.06 mm away from the tip of the corrosion groove, and the hydrogen accumulation became the maximum. It was analytically found that the SSC crack initiated and propagated with HE mechanism dominated type when the threshold value of about 0.82 ppm is exceeded.

    DOI: 10.2355/isijinternational.isijint-2022-236

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  • Evaluation of Cleavage Fracture Behavior of C14 Fe2W Laves Phase by First-principles Calculations and Crystal Orientation Analysis

    Yamasaki, S; Morikawa, T; Tanaka, M; Watanabe, Y; Yamashita, M; Izumi, S

    ISIJ International   62 ( 10 )   2118 - 2125   2022年10月   ISSN:09151559 eISSN:13475460

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    記述言語:その他   掲載種別:研究論文(学術雑誌)   出版者・発行元:一般社団法人 日本鉄鋼協会  

    In this study, the cleavage fracture of the C14 Fe2W Laves phase was investigated by first-principles calculations and crystal orientation analysis using scanning electron microscopy. Trace analysis of the orientations of cleavage planes revealed that cleavage fracture occurred in five types of crystal planes: (0001), {1100}, {1120}, {1101}, and {1122}. Among these fractures, the fracture at (0001) is the most preferable. From, the first-principle calculations of the surface energy for fracture, Young’s modulus, and Poisson’s ratio, the minimum fracture toughness value of 1.62 MPa·m1/2 was obtained at (0001). The tendency of the calculated fracture toughness to become larger with high indexed planes is almost the same as the frequency of the types of cleavage planes in the trace analysis. It was concluded that the fracture toughness of the C14 Fe2W Laves phase is controlled by the surface energy for fracture and Young’s modulus.

    DOI: 10.2355/isijinternational.isijint-2022-122

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  • LPSO型Mg合金のキンク形成観察とキンク導入加工プロセスの最適化

    光原 昌寿, 山﨑 重人, 安藤 大輔

    まてりあ   61 ( 9 )   543 - 549   2022年9月   ISSN:13402625 eISSN:18845843

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    記述言語:日本語   出版者・発行元:公益社団法人 日本金属学会  

    DOI: 10.2320/materia.61.543

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  • 低合金鋼ラインパイプの低H2S濃度サワー環境下における硫化物応力腐食割れ挙動 査読

    嶋村 純二, 森川 龍哉, 山﨑 重人, 田中 將己

    鉄と鋼   108 ( 9 )   642 - 655   2022年9月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    DOI: https://doi.org/10.2355/tetsutohagane.TETSU-2022-013

  • レーザ積層造形法と電子ビーム積層造形法で作製したAC8Aアルミニウム合金のミクロ組織と引張特性

    安達 充, 奥平 有, 山﨑 重人, 光原 昌寿, 中島 英治, 小岩井 修二, 橋詰 良樹, 村上 勇夫, 寺田 大将

    軽金属   72 ( 5 )   206 - 213   2022年5月   ISSN:04515994 eISSN:18808018

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    記述言語:日本語   出版者・発行元:一般社団法人 軽金属学会  

    The mechanical properties of JISAC8A alloys (Al-12%Si-1%Mg-1%Ni-1%Cu alloy) fabricated by laser-based powder bed fusion (LB) or electron-based powder bed fusion (EB) or gravity casting (CAST) were studied by means of tensile tests at room temperature and 300°C. These alloys were under two types of heat-treatment sequences. One was a T6 treatment, which was corresponding to the heat treatment at 500°C for 2h and 170°C for 4 h, followed by the annealing at 300°C for 10 h. Another was directly annealed at 300°C for 10 h after the fabrication. In the annealed specimens without T6 treatment, the LB alloy showed the highest strength and best elongation at room temperature and 300°C, because eutectic Si particles and Al-Ni-Cu-Fe compounds formed very fine network structure in Al matrix. In the annealed specimens with T6 treatment, the tensile strength at room temperature did not depend on the fabrication methods but the LB alloy showed the best elongation because of finer and isotropic shape of secondary phase particles. The annealed CAST alloy showed the highest strength at 300°C, and the annealed LB alloy showed the lowest strength at 300°C.

    DOI: 10.2464/jilm.72.206

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  • レーザ積層造形法と電子ビーム積層造形法で作製したAC8A アルミニウム合金のミクロ組織と引張特性 査読

    安達 充, 奥平 有, 山﨑 重人, 光原 昌寿, 中島 英治, 小岩井 修二, 橋詰 良樹, 村上 勇夫, 寺田 大将

    軽金属   72 ( 5 )   206 - 213   2022年5月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    DOI: https://doi.org/10.2464/jilm.72.206

  • 低合金鋼ラインパイプの低H<sub>2</sub>S濃度サワー環境下における硫化物応力腐食割れ挙動

    嶋村 純二, 森川 龍哉, 山﨑 重人, 田中 將己

    鉄と鋼   108 ( 9 )   642 - 655   2022年   ISSN:00211575 eISSN:18832954

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    記述言語:日本語   出版者・発行元:一般社団法人 日本鉄鋼協会  

    Resistance to Sulfide Stress Cracking (SSC) caused by local hard zones of pipe inner surface has been required in low alloy linepipe steel. In this study, using two samples with different surface hardness, the detailed SSC initiation behavior was clarified by four-point bend (4PB) SSC tests in which immersion time and applied stress were changed in a sour environment containing 0.15 bar hydrogen sulfide (H2S) gas. SSC cracks occurred when the applied stress was higher than 90% actual yield strength (AYS) in higher surface hardness samples over 270 HV0.1. From the fracture surface observation of SSC crack sample, it was found that the mechanism gradually shifted from active path corrosion (APC) to hydrogen embrittlement (HE), and that the influence of APC mechanism remained partially in the process of SSC initiation at the tip of corrosion pit or groove. The polarization measurement in the 4PB SSC test showed that the anodic and cathodic reactions (especially cathodic reactions) were activated when the applied stress was 90% AYS or higher. The FEM coupled analysis simulating the stress and strain concentration at the bottom tip of the corrosion groove and the hydrogen diffusion and accumulation was carried out. The principal stress in the tensile direction showed the maximum value at 0.04-0.06 mm away from the tip of the corrosion groove, and the hydrogen accumulation became the maximum. It was analytically found that the SSC crack initiated and propagated with HE mechanism dominated type when the threshold value of about 0.82 ppm is exceeded.

    DOI: 10.2355/tetsutohagane.tetsu-2022-013

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  • Effects of temperature and grain size on active twinning systems in commercially pure titanium

    Genki Tsukamoto, Tomonori Kunieda, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Journal of Alloys and Compounds   884   2021年12月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    In order to clarify the effects of grain boundary, grain size and deformation temperature on twinning deformation in polycrystalline commercially pure titanium, active twinning systems during compression deformation at temperatures from 25 °C to 800 °C investigated using SEM/EBSD techniques. Four twinning systems were confirmed to operate under compression at 10% strain in a deformation temperature dependent manner: {112̅1} and {112̅2} twins were observed only at relatively low temperatures (e.g. ≦ 400 °C), while, {101̅1} twins were observed at relatively high temperatures (e.g. ≧ 400 °C), and {101̅2} twins formed at every tested temperature (25 °C–800 °C). Our results suggested that the effects of strain concentration at grain boundaries on twinning differ based on the active twinning systems, which are affected by: 1) the difference in the formation temperature ranges between single-crystal and polycrystalline specimens, 2) the ratio of the number of deformation twins touching grain boundaries to the total number of deformation twins, and 3) grain size dependence.

    DOI: 10.1016/j.jallcom.2021.161154

  • Evaluation of cleavage fracture behavior of C14 Fe<inf>2</inf>W laves phase by first principle calculation and crystal orientation analysis

    Shigeto Yamasaki, Masaki Tanaka, Tatsuya Morikawa, Yasuaki Watanabe, Mitsuo Yamashita, Sakae Izumi

    Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan   107 ( 11 )   977 - 985   2021年11月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    Cleavage fracture of C14 Fe2W Laves phase was investigated using crystal orientation measurement with scanning electron microscopy and first-principles calculations. Trace analysis of the orientations of cleavage planes reveals that cleavage fracture occurred at five types of crystal planes of (0001), {1100}, {1120}, {1101} and {1122}, among which the fracture at (0001) is the most preferable. The first-principle calculations of the surface energy for fracture, Young's modulus, and Poisson's ratio showed that the minimum fracture toughness value of 1.62 MPa·m1/2 was obtained at (0001). The tendency that the values of calculated fracture toughness become larger with the higher indexed planes is almost the same as the frequency of the types of cleavage planes in the trace analysis. It is concluded that the fracture toughness of C14 Fe2W Laves phase is controlled by the surface energy for fracture and Young’s modulus.

    DOI: 10.2355/tetsutohagane.TETSU-2021-069

  • Persistent slip observed in TiZrNbHfTa: A body-centered high-entropy cubic alloy 査読 国際誌

    Tanaka, M., Okajo, S., Yamasaki, S. & Morikawa, T.

    Scripta Materialia   2021年7月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • Persistent slip observed in TiZrNbHfTa: A body-centered high-entropy cubic alloy

    Masaki Tanaka, Shinji Okajo, Shigeto Yamasaki, Tatsuya Morikawa

    Scripta Materialia   200   2021年7月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    Slip properties of TiZrNbHfTa were evaluated to obtain ψ–χ relationships, where χ is defined as the angle between the maximum shear stress plane and (1¯01). ψ is defined as the angle between the apparent slip plane and (1¯01). Bending tests were conducted with micrometer-sized cantilevers fabricated from a single grain with a focused ion beam. Slip bands appear to be straight on a micrometer length-scale, as for Fe–Si alloys, which suggests a persistent slip. However, the ψ–χ relationship indicated that ψ is nearly the same as χ, suggesting that there is no persistent slip. Detailed observations with an atomic force microscope confirm that cross-slipping is so frequent at a sub-micrometer length-scale that the slip bands appear to be straight and the maximum shear stress plane is observed on a micrometer length-scale. Here, TiZrNbHfTa shows abnormally frequent cross-slipping, which is a novel characteristic of high-entropy body-centered cubic alloys.

    DOI: 10.1016/j.scriptamat.2021.113895

  • Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method

    Shigeto Yamasaki, Misaki Deguchi, Masatoshi Mitsuhara, Hideharu Nakashima, Yutaro Ota, Keiji Kubushiro

    Microscopy   70 ( 3 )   265 - 277   2021年6月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.

    DOI: 10.1093/jmicro/dfaa060

  • Quantitative analysis of the Portevin–Le Chatelier effect by combining digital image correlation and dead-weight-type tensile test

    Shigeto Yamasaki, Tomoki Miike, Masatoshi Mitsuhara, Hideharu Nakashima, Ryutaro Akiyoshi, Takahiko Nakamura, Shimpei Kimura

    Materials Science and Engineering A   816   2021年6月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    A quantitative evaluation method of a serration deformation behavior by a dead-weight tensile test combined with a strain measurement by a DIC method is proposed. This method applies to binary solid solution aluminum alloys and a ternary cluster strengthened aluminum alloy. In the dead-weight tensile test, the serrated flow was measured as a stress-strain curve with a stepped-shape divided into two stages of a stress rising phase and a strain burst phase. By adopting this tensile test, the serration deformation behavior can be measured with an extremely reproducibility. It was confirmed that an elastic deformation occurs predominantly in the stress rising phase, and this deformation behavior is discussed in relation to the concentration of solid solution elements. Propagation of PLC bands has occurred in the strain burst phase. An activation volume obtained from the strain rate in the PLC bands was in good agreement with a calculated value based on a distribution interval assuming a regular square distribution of solute elements. For the ternary alloy strengthened by clusters, it is also shown that this method can be applied to the qualitative estimation of the change in the residual amount of the solid solution element in the matrix during natural aging.

    DOI: 10.1016/j.msea.2021.141277

  • Generalized Slip Operation Factor Considering Contribution of Secondary Slip Systems 査読 国際誌

    Kawano, Y., Mayama, T., Mitsuhara, M., Yamasaki, S. & Sato, M.

    Materials Today Communications   2021年3月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

  • Generalized Slip Operation Factor Considering Contribution of Secondary Slip Systems

    Yoshiki Kawano, Tsuyoshi Mayama, Masatoshi Mitsuhara, Shigeto Yamasaki, Michihiro Sato

    Materials Today Communications   26   2021年3月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    Slip operation factor (SOF), which considers the effect of mechanical interactions between plastically “soft” and “hard” regions, is a function of the Schmid factor (SF) and critical resolved shear stress (CRSS). It is used as an indicator to efficiently predict the ease of slip operation of metal materials at the grain level. While SOF could predict strain distributions, it was not compliant to the prediction of those for individual slip systems. Additionally, the contribution of secondary slip systems was disregarded in the SOF. In this study, the SOF was first extended to adapt to individual slip systems. This extended and generalized form of the SOF was called SOFS. Next, the contribution of secondary slip systems was considered in SOF, where the modified version of the SOF was called MSOF. Polycrystalline α-Ti models were built from crystal orientation maps obtained by electron back-scattered diffraction (EBSD), and the strain distributions under uniaxial tensile loading were predicted using the SOF, SOFS, and MSOF. The results obtained were compared with those obtained via crystal plasticity finite element (CPFE) analysis. The distributions obtained by the SOFS were similar to slip strain distributions for individual slip systems when single slips were dominant and the deformation was slight. The MSOF also successfully predicted the strain distributions with higher accuracy than that offered by the SOF.

    DOI: 10.1016/j.mtcomm.2021.102041

  • One-trillionth level toluene detection using a dual-designed semiconductor gas sensor: Material and sensor-driven designs

    Koichi Suematsu, Wataru Harano, Shigeto Yamasaki, Ken Watanabe, Kengo Shimanoe

    ACS Applied Electronic Materials   2 ( 12 )   4122 - 4126   2020年12月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    Lowering the volatile organic compound (VOC) gas detection limit toward the ppt level on a resistive-type semiconductor gas sensor was achieved by combining the material and sensor-driven designs. We fabricated Pd-SnO2 clustered nanoparticles, a material that is highly sensitive to VOC gas, on a microsensor device with a double-pulse-driven mode. This mode was involved in switching the heater-on periods at high-temperature preheating and measurement phases and the rest phase during a heater-off period between preheating and measurement phases. The electrical resistance in synthetic air and the sensor response to toluene increased as preheating temperatures increased because of an increase in the amount of O2− adsorbed on the particle surface. In addition, extending the rest time between the preheating and measurement phases significantly improved the sensor response to toluene. According to the relationship between the sensor response and toluene concentration, we improved the lower detection limit for toluene gas to below 10 ppt, with preheating and measurement temperatures at 400 and 250 °C, respectively, and rest time at 100 s. Therefore, the combination of the material and sensor-driven designs may play a key role in improving the sensor performance.

    DOI: 10.1021/acsaelm.0c00902

  • Relationship between Creep Strength and Magnetic Properties of Cobalt-bearing High Chromium Ferritic Steel

    Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    TETSU TO HAGANE-JOURNAL OF THE IRON AND STEEL INSTITUTE OF JAPAN   106 ( 11 )   12 - 22   2020年11月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    In this study, the relation between the change of the magnetic properties and the creep strength with the addition of Co was investigated for ferritic steel containing 15 mass%Cr. Co addition up to 6 mass% hardly contributes to solid solution strengthening and precipitation strengthening at room temperature. However, in the range of 650 degrees C to 750 degrees C, it was confirmed that the addition of Co was effective for the creep strengthening because the steel with a larger amount of Co had higher creep strength. This creep strengthening is explained by a reduction in the diffusion rate associated with a change in magnetic properties by Co addition. The increase of the volume magnetization of the steel with increase of Co amount in the temperature range from room temperature to about 800 degrees C was confirmed. Comparing the difference in volume magnetization and the ratio of creep strain rate for steels with different amounts of Co, a clear correlation was found between the values. That is, at the temperature at which the difference in volume magnetization becomes maximum, the peak of the creep strain rate ratio was observed. This result is explained as follows. In a low temperature region where the magnetization is large or in a high temperature region above the Curie point of both steels, there is no significant difference in the creep strength between them. However, in the temperature where one steel loses the ferromagnetism but the other steel maintains ferromagnetism, a significant difference in the creep strength was observed.

    DOI: 10.2355/tetsutohagane.TETSU-2020-041

  • One-trillionth level toluene detection using a dual-designed semiconductor gas sensor: Material and sensor-driven designs 査読 国際誌

    Suematsu, K., Harano, W., Yamasaki, S., Watanabe, K. & Shimanoe, K.

    ACS Applied Electronic Materials   2020年11月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

  • Dislocation motion and microstructure evolution deformed during creep at room temperature in Ti-6Al-4V alloy

    Misaki Deguchi, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima, Yutaro Ota

    Keikinzoku/Journal of Japan Institute of Light Metals   70 ( 8 )   405 - 414   2020年10月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    The deformation behavior and microstructure evolution of Ti-6Al-4V alloy under room temperature creep was investigated using mechanical test and scanning electron microscope observation with electron back-scatter diffraction method. The alloys were creep deformed and ruptured under initial stresses of 874 MPa, 889 MPa and 904 MPa at room temperature. The rapid stress change test revealed that creep deformation was controlled by the viscous slip motion of dislocations. The stress exponent was estimated as 59. The strain rate of acceleration creep region calculated by the Norton's law with the high stress exponent was inconsistent with that measured by the experimental creep test. Using the slip trace analysis, it was found that single dislocation slip in basal and prism were mainly activated in the early stage of creep, and multiple slips were often observed as the deformation progresses. Especially, the multiple slip including 1st pyramidal slip believed to be effective for suppressing strain rate acceleration in creep. In addition, the work hardening behavior during creep showed a strain rate dependence, indicating that the lower the strain rate is, the more work hardening occurs.

    DOI: 10.2464/JILM.70.405

  • Morphological and crystallographic features of kink bands in long-period stacking ordered Mg-Zn-Y alloy analyzed by serial sectioning SEM-EBSD observation method 査読 国際誌

    Tsubasa Tokuzumi, Shigeto Yamasaki, Wansong Li, Masatoshi Mitsuhara, Hideharu Nakashima

    Materialia   12   100716   2020年8月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: https://doi.org/10.1016/j.mtla.2020.100716

  • Morphological and crystallographic features of kink bands in long-period stacking ordered Mg-Zn-Y alloy analyzed by serial sectioning SEM-EBSD observation method

    Tsubasa Tokuzumi, Shigeto Yamasaki, Wansong Li, Masatoshi Mitsuhara, Hideharu Nakashima

    Materialia   12   2020年8月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    © 2020 Acta Materialia Inc. We investigated the pseudo three-dimensional features of kink bands formed by the compression deformation of a directionally solidified Mg85Zn6Y9 alloy. The kink bands of interest included ridge kinks with clear surface relief and gentle kinks with almost no surface relief. Observation of surface undulation by laser microscopy and electron backscatter diffraction with serial sectioning by mechanical polishing revealed the pseudo three-dimensional morphology and crystal rotation of these kink bands. The features of the observed kink bands are explained by a pseudo three-dimensional arrangement of disclination lines.

    DOI: 10.1016/j.mtla.2020.100716

  • Kink Formation Process in Long-Period Stacking Ordered Mg-Zn-Y Alloy

    Shigeto Yamasaki, Tsubasa Tokuzumi, Wansong Li, Masatoshi Mitsuhara, Koji Hagihara, Toshiyuki Fujii, Hideharu Nakashima

    Acta Materialia   195   25 - 34   2020年8月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    © 2020 Acta Materialia Inc. The formation process of the kink bands in a directionally solidified, polycrystalline, long-period stacking ordered (LPSO) Mg85Zn6Y9 phase during compression deformation was investigated. In-situ compression observations by scanning electron microscopy and electron backscattered diffraction analysis revealed that regions with localized crystal orientation rotation appeared before ridge kinks formed as surface relief. In this paper, it is called as pre-kink The observed pre-kinks were composed of two separate regions rotated in opposite directions to each other and distinguished from one another by the three boundaries. A transmission electron microscopy observation revealed that the boundaries of the pre-kink are sub-boundaries consisting of edge dislocation array, and both its ends are terminated within the matrix. These characteristics match the reported that of regular ridge kink boundaries. In addition, while pre-kinks do not possess the ability of complete reversibility, its boundaries are capable of moving elastically.

    DOI: 10.1016/j.actamat.2020.04.051

  • Ti-6Al-4V 合金における室温クリープ中の転位の運動様式と変形組織の発達過程 査読

    Deguchi, M., Yamasaki, S., Mitsuhara, M., Nakashima, H. & Ota, Y.

    軽金属   2020年8月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

  • In situ EBSD study of deformation behavior of primary α phase in a bimodal Ti-6Al-4V alloy during uniaxial tensile tests 査読

    Wansong Li, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Materials Characterization   163   2020年5月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1016/j.matchar.2020.110282

  • In situ EBSD study of deformation behavior of primary α phase in a bimodal Ti-6Al-4V alloy during uniaxial tensile tests

    Wansong Li, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Materials Characterization   163   2020年5月

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    記述言語:その他   掲載種別:研究論文(学術雑誌)  

    © 2020 Elsevier Inc. Uniaxial tension experiments and electron backscatter diffraction were performed on a bimodal Ti-6Al-4V alloy to study in situ the deformation behavior of primary hcp-Ti (αp). It was found that the strain could be accommodated by the activation of slip systems and by grain rotations. The prismatic slip was the primary slip mode of the αp. From the analysis of kernel average misorientation and geometrically necessary dislocation, it was shown that the dislocations mainly distributed in the vicinity of grain and sub-grain boundaries, and part of the dislocations distributed around slip lines. It was the dislocation activities that led to the formation of the low angle grain boundary and its transformation to the high angle grain boundary. It's important that tracking of deformation heterogeneities with significance to performance. By analyzing the rotation angle, average rotation rate, and rotation path of grains, it was shown that grain rotation heterogeneity occurred during the deformation. From the observation of the loading direction, grain rotation paths kept with the texture evolution direction of all αp. The grains activated in the basal slip gradually rotated to the ⟨101¯1⟩ pole and enhanced the intensity of the ⟨101¯1⟩ texture. Meanwhile, the grains activated in prismatic or 1st-order pyramidal slip rotated to the ⟨101¯0⟩ pole and enhanced the intensity of the ⟨101¯0⟩ texture. Grain rotation and texture evolution are related to mechanical properties.

    DOI: 10.1016/j.matchar.2020.110282

  • Electron tomography imaging methods with diffraction contrast for materials research 招待 査読 国際誌

    Satoshi Hata, Hiromitsu Furukawa, Takashi Gondo, Daisuke Hirakami, Noritaka Horii, Ken Ichi Ikeda, Katsumi Kawamoto, Kosuke Kimura, Syo Matsumura, Masatoshi Mitsuhara, Hiroya Miyazaki, Shinsuke Miyazaki, Mitsu Mitsuhiro Murayama, Hideharu Nakashima, Hikaru Saito, Masashi Sakamoto, Shigeto Yamasaki

    Microscopy   69 ( 3 )   141 - 155   2020年5月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1093/jmicro/dfaa002

  • Electron tomography imaging methods with diffraction contrast for materials research 招待 査読 国際誌

    Satoshi Hata, Hiromitsu Furukawa, Takashi Gondo, Daisuke Hirakami, Noritaka Horii, Ken Ichi Ikeda, Katsumi Kawamoto, Kosuke Kimura, Syo Matsumura, Masatoshi Mitsuhara, Hiroya Miyazaki, Shinsuke Miyazaki, Mitsu Mitsuhiro Murayama, Hideharu Nakashima, Hikaru Saito, Masashi Sakamoto, Shigeto Yamasaki

    Microscopy   69 ( 3 )   141 - 155   2020年3月

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    記述言語:英語  

    © 2020 The Author(s). Published by Oxford University Press on behalf of The Japanese Society of Microscopy. All rights reserved. Transmission electron microscopy (TEM) and scanning transmission electron microscopy (STEM) enable the visualization of three-dimensional (3D) microstructures ranging from atomic to micrometer scales using 3D reconstruction techniques based on computed tomography algorithms. This 3D microscopy method is called electron tomography (ET) and has been utilized in the fields of materials science and engineering for more than two decades. Although atomic resolution is one of the current topics in ET research, the development and deployment of intermediate-resolution (non-atomic-resolution) ET imaging methods have garnered considerable attention from researchers. This research trend is probably not irrelevant due to the fact that the spatial resolution and functionality of 3D imaging methods of scanning electron microscopy (SEM) and X-ray microscopy have come to overlap with those of ET. In other words, there may be multiple ways to carry out 3D visualization using different microscopy methods for nanometer-scale objects in materials. From the above standpoint, this review paper aims to (i) describe the current status and issues of intermediate-resolution ET with regard to enhancing the effectiveness of TEM/STEM imaging and (ii) discuss promising applications of state-of-the-art intermediate-resolution ET for materials research with a particular focus on diffraction contrast ET for crystalline microstructures (superlattice domains and dislocations) including a demonstration of in situ dislocation tomography.

    DOI: 10.1093/jmicro/dfaa002

  • Quantitative evaluation of slip activity in polycrystalline α-titanium considering non-local interactions between crystal grains 査読

    Yoshiki Kawano, Michihiro Sato, Tsuyoshi Mayama, Masatoshi Mitsuhara, Shigeto Yamasaki

    International Journal of Plasticity   127   2020年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1016/j.ijplas.2019.12.001

  • Effect of Fe addition on heat-resistant aluminum alloys produced by selective laser melting

    Shigeto Yamasaki, Tomo Okuhira, Masatoshi Mitsuhara, Hideharu Nakashima, Jun Kusui, Mitsuru Adachi

    Metals   9 ( 4 )   2019年4月

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    記述言語:その他  

    © 2019 by the authors. Licensee MDPI, Basel, Switzerland. The effect of Fe addition on the high-temperature mechanical properties of heat-resistant aluminum alloys produced by selective laser melting (SLM) was investigated in relation to the alloy microstructures. Fe is generally detrimental to the properties of cast aluminum alloys; however, we found that Fe-containing alloys produced by SLM had improved high-temperature strength and good ductility. Microstructural observations revealed that the increase in the high-temperature strength of the alloys was due to the dispersion of fine rod-shaped Fe-Si-Ni particles unique to the SLM material instead of the cell-like structure of eutectic Si.

    DOI: 10.3390/met9040468

  • Controlled Growth of Large-Area Uniform Multilayer Hexagonal Boron Nitride as an Effective 2D Substrate 査読

    Yuki Uchida, Sho Nakandakari, Kenji Kawahara, Shigeto Yamasaki, Masatoshi Mitsuhara, Hiroki Ago

    ACS Nano   12 ( 6 )   6236 - 6244   2018年6月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    © Copyright 2018 American Chemical Society. Multilayer hexagonal boron nitride (h-BN) is an ideal insulator for two-dimensional (2D) materials, such as graphene and transition metal dichalcogenides, because h-BN screens out influences from surroundings, allowing one to observe intrinsic physical properties of the 2D materials. However, the synthesis of large and uniform multilayer h-BN is still very challenging because it is difficult to control the segregation process of B and N atoms from metal catalysts during chemical vapor deposition (CVD) growth. Here, we demonstrate CVD growth of multilayer h-BN with high uniformity by using the Ni-Fe alloy film and borazine (B3H6N3) as catalyst and precursor, respectively. Combining Ni and Fe metals tunes the solubilities of B and N atoms and, at the same time, allows one to engineer the metal crystallinity, which stimulates the uniform segregation of multilayer h-BN. Furthermore, we demonstrate that triangular WS2 grains grown on the h-BN show photoluminescence stronger than that grown on a bare SiO2 substrate. The PL line width of WS2/h-BN (the minimum and mean widths are 24 and 43 meV, respectively) is much narrower than those of WS2/SiO2 (44 and 67 meV), indicating the effectiveness of our CVD-grown multilayer h-BN as an insulating layer. Large-area, multilayer h-BN realized in this work will provide an excellent platform for developing practical applications of 2D materials.

    DOI: 10.1021/acsnano.8b03055

  • Controlled Growth of Large-Area Uniform Multilayer Hexagonal Boron Nitride as an Effective 2D Substrate 査読

    Yuki Uchida, Sho Nakandakari, Kenji Kawahara, Shigeto Yamasaki, Masatoshi Mitsuhara, Hiroki Ago

    ACS nano   12 ( 6 )   6236 - 6244   2018年6月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1021/acsnano.8b03055

  • Effect of Bi or Sb addition on high temperature deformation behavior in Sn-Cu-Ni solder alloys 査読

    Masayuki Takano, Keiji Kuroda, Kohei Hase, Shuuto Tanaka, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals   81 ( 11 )   502 - 509   2017年9月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/jinstmet.J2017025

  • Effect of Bi or Sb addition on high temperature deformation behavior in Sn-Cu-Ni solder alloys 査読

    Masayuki Takano, Keiji Kuroda, Kohei Hase, Shuuto Tanaka, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals   81 ( 11 )   502 - 509   2017年9月

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    記述言語:日本語   掲載種別:研究論文(学術雑誌)  

    © 2017 The Japan Institute of Metals and Materials. Global concerns over the environmental impact and health effects of the lead-based solders have led to the development of lead-free solder alloys. Further improvements in the reliability of lead-free solder alloys at high temperatures are required for downsizing of electronic components in vehicles. In this work, tensile and creep tests and microstructure analysis were carried out to determine the effect of Bi or Sb addition on high-temperature deformation behavior in Sn-Cu-Ni solder alloys. The addition of Bi or Sb increased the strength of the Sn-Cu-Ni solder alloys. The stress exponent was estimated to be ≥3, indicating that the high- Temperature deformation was controlled by dislocation creep. Furthermore, in both the alloys, the stress exponent observed in the low stress region was nearly equal to 3 and discontinuously increased to ≥7 in the high stress region. For Sb addition, the solute atmosphere drag mechanism was observed in the low stress region.

    DOI: 10.2320/jinstmet.J2017025

  • Multiscale in situ deformation experiments A sequential process from strain localization to failure in a laminated Ti-6Al-4V alloy 査読

    Motomichi Koyama, Keita Yamanouchi, Qinghua Wang, Shien Ri, Yoshihisa Tanaka, Yasuaki Hamano, Shigeto Yamasaki, Masatoshi Mitsuhara, Masataka Ohkubo, Hiroshi Noguchi, Kaneaki Tsuzaki

    Materials Characterization   128   217 - 225   2017年6月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1016/j.matchar.2017.04.010

  • Multiscale in situ deformation experiments: A sequential process from strain localization to failure in a laminated Ti-6Al-4V alloy 査読

    Motomichi Koyama, Keita Yamanouchi, Qinghua Wang, Shien Ri, Yoshihisa Tanaka, Yasuaki Hamano, Shigeto Yamasaki, Masatoshi Mitsuhara, Masataka Ohkubo, Hiroshi Noguchi, Kaneaki Tsuzaki

    Materials Characterization   128   217 - 225   2017年6月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    © 2017 Elsevier Inc. The microscopic factors causing tensile failure of an α/β laminated Ti-6Al-4V alloy were investigated through in situ scanning electron microscopy and sampling moiré at an ambient temperature. Specifically, multiscale in situ microscopic observations were conducted to extract the most crucial factor of the failure. Slip localization in the vicinity of an intergranular α-sheet was clarified to be the primary factor that causes failure of the Ti-6Al-4V alloy. In addition, no relationship between interfacial strain localization and macroscopic shear localization at 45 degrees against the tensile direction was observed.

    DOI: 10.1016/j.matchar.2017.04.010

  • Effect of Cu and Ni addition on high temperature deformation behavior in Sn-Cu-Ni solder alloys 査読

    Masayuki Takano, Keiji Kuroda, Kohei Hase, Shuuto Tanaka, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima

    Nippon Kinzoku Gakkaishi/Journal of the Japan Institute of Metals   81 ( 7 )   337 - 344   2017年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/jinstmet.J2016069

  • Microstructure and creep property in polycrystalline Ni-based alloy with intergranular intermetallics 査読

    Takanori Ito, Shigeto Yamasaki, Masatoshi Mitsuhara, Hideharu Nakashima, Minoru Nishida, Mitsuharu Yonemura

    Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan   103 ( 7 )   434 - 442   2017年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2355/tetsutohagane.TETSU-2016-107

  • Effect of intergranular carbides on creep strength in nickel-based heat-resistant alloys 査読

    Takanori Ito, Shigeto Yamasaki, Masatoshi Mitsuhara, Minoru Nishida, Mitsuharu Yonemura

    Materials Transactions   58 ( 1 )   52 - 58   2017年1月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/matertrans.M2016291

  • Creep strengthening by lath boundaries in 9Cr ferritic heat-resistant steel 査読

    Masatoshi Mitsuhara, Shigeto Yamasaki, Masaki Miake, Hideharu Nakashima, Minoru Nishida, Junichi Kusumoto, Akihiro Kanaya

    Philosophical Magazine Letters   96 ( 2 )   76 - 83   2016年2月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.1080/09500839.2016.1154200

  • Creep strengthening by lath boundaries in 9Cr ferritic heat-resistant steel 査読

    Masatoshi Mitsuhara, Shigeto Yamasaki, Masaki Miake, Hideharu Nakashima, Minoru Nishida, Junichi Kusumoto, Akihiro Kanaya

    Philosophical Magazine Letters   96 ( 2 )   76 - 83   2016年2月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    © 2016 Taylor and Francis. The interactions between dislocations and lath boundaries in Grade 91 steel were observed by an in situ transmission electron microscopy tensile test at 973 K. Dislocations glided slowly and bowed out in a martensite lath interior. The ends of the dislocation were connected to the lath boundaries. In a tempered specimen, the pinning stress caused by the lath boundary was estimated to be >70 MPa with a lath width of 0.4 m. In crept specimens, lath coarsening reduced the pinning effect.

    DOI: 10.1080/09500839.2016.1154200

  • 3D visualization of dislocation arrangement using scanning electron microscope serial sectioning method 査読

    S. Yamasaki, M. Mitsuhara, K. Ikeda, S. Hata, H. Nakashima

    Scripta Materialia   101   80 - 83   2015年5月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    © 2015 Acta Materialia Inc. Published by Elsevier Ltd. We performed the three-dimensional visualization of dislocations through serial sectioning and use of SEM electron channeling contrast (ECC) images for a crept nickel-based alloy. We successfully reconstructed a volume of approximately 7.5 μm3, including dislocation arrangements, by performing calculations based on the continuous tomograms of ECC images. By incorporating the information on crystal orientation obtained by the electron back-scattered diffraction, we verified that the three-dimensional arrangement of dislocations, such as slip plane, was accurately reflected in the three-dimensional volume.

    DOI: 10.1016/j.scriptamat.2015.02.001

  • 純ニッケルの極低ひずみ速度クリープの変形機構の解明

    小池幸司, 山崎重人, 池田賢一, 波多聰, 中島英治

    日本金属学会講演概要(CD-ROM)   153rd   ROMBUNNO.P124   2013年9月

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    記述言語:日本語  

    純ニッケルの極低ひずみ速度クリープの変形機構の解明

  • オーステナイト系耐熱鋼の局所結晶方位解析によるクリープひずみの評価

    山崎重人, 光原昌寿, 池田賢一, 波多聰, 中島英治

    材料とプロセス(CD-ROM)   26 ( 1 )   ROMBUNNO.258   2013年3月

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    記述言語:日本語  

    オーステナイト系耐熱鋼の局所結晶方位解析によるクリープひずみの評価

  • SEM/EBSD法によるクリープ変形に伴うGr.92鋼溶接継手の組織変化挙動解析

    光原昌寿, 市瀬祐輔, 市瀬祐輔, 山崎重人, 池田賢一, 波多聰, 中島英治, 長谷川泰士

    材料とプロセス(CD-ROM)   25 ( 2 )   ROMBUNNO.266   2012年9月

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    記述言語:日本語  

    SEM/EBSD法によるクリープ変形に伴うGr.92鋼溶接継手の組織変化挙動解析

  • フェライト系耐熱鋼の低応力クリープ変形挙動

    山崎重人, 池田賢一, 波多聰, 中島英治

    日本金属学会講演概要(CD-ROM)   150th   ROMBUNNO.528   2012年3月

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    記述言語:日本語  

    フェライト系耐熱鋼の低応力クリープ変形挙動

  • 局所方位解析法を用いたフェライト系耐熱鋼溶接熱影響部クリープ弱化要因の特定

    市瀬祐輔, 山崎重人, 光原昌寿, 池田賢一, 波多聰, 中島英治, 長谷川泰士

    日本金属学会講演概要(CD-ROM)   149th   ROMBUNNO.POSUTASESSHON,439   2011年10月

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    記述言語:日本語  

    局所方位解析法を用いたフェライト系耐熱鋼溶接熱影響部クリープ弱化要因の特定

  • Low-temperature creep at ultra-low strain rates in pure aluminum studied by a helicoid spring specimen technique 査読

    Junjie Shen, Shigeto Yamasaki, Ken Ichi Ikeda, Satoshi Hata, Hideharu Nakashima

    Materials Transactions   52 ( 7 )   1381 - 1387   2011年7月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    DOI: 10.2320/matertrans.M2010405

  • 酸化物分散強化型9Crフェライト系耐熱鋼の3次元組織と高温強度

    光原 昌寿, 原田 絵梨香, 山崎 重人, 池田 賢一, 波多 聰, 中島 英治, 大塚 智史, 皆藤 威二

    可視化情報学会誌 = Journal of the Visualization Society of Japan   31 ( 122 )   98 - 103   2011年7月

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    記述言語:日本語  

    高速増殖炉内燃料被覆管の候補材料として研究開発が行われている酸化物分散強化(ODS)型9Crフェライト系耐熱鋼について,内部に生成するイットリア系酸化物の分散状態を電子線トモグラフィーにより3次元的に評価した.酸化物は,高密度な領域と低密度な領域が鋼管の押出し方向と平行になるように積層した分布を持っていた.それぞれの領域で,酸化物による変形への抵抗力を粒径や粒子間距離などから算出すると,700℃において,高密度領域では232~278MPa,低密度領域では154~184MPaであった.さらに,クリープ特性を評価したところ,約140MPaでクリープ変形機構の遷移が認められた.このしきい値は,低密度領域の酸化物による変形の抵抗力におおよそ一致している.すなわち,低密度に酸化物が分散した領域において転位の運動が速く,このことがODS鋼の高温強度や変形機構に強く影響を及ぼしていると示唆された.

    DOI: 10.3154/jvs.31.98

  • Low-temperature creep at ultra-low strain rates in pure aluminum studied by a helicoid spring specimen technique 査読

    Junjie Shen, Shigeto Yamasaki, Ken Ichi Ikeda, Satoshi Hata, Hideharu Nakashima

    Materials Transactions   52 ( 7 )   1381 - 1387   2011年7月

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    記述言語:英語   掲載種別:研究論文(学術雑誌)  

    The creep behavior in pure aluminum has been investigated by helicoid spring creep tests at strain rates, ε̇, lower than 10-10 s-1 and low temperature ranging from 0.32Tm to 0.43T m. It was found that the creep behavior in this region depends strongly on grain sizes and impurity concentrations. For high-purity aluminum (5 N Al) with an average grain size, dg > 1600 μm, nearly the wire diameter of the spring sample, where the role of grain boundary during creep deformation can be negligible, the stress exponent was n ∼ 5 and the activation energy was Qc = 32 kJ/mol. Microstructural observation showed the formation of large dislocation cells (∼10μm) and tangled dislocations at the cell walls. For high-purity aluminum (5N Al) with d g = 24 μm, the stress exponent was n ∼ 1 and the activation energy was Qc = 15kJ/mol. On the other hand, for commercial low-purity aluminum (2 N Al) with dg = 25 μm, the stress exponent was n = 2 and the activation energy was Qc = 25 kJ/mol. Microstructural observations revealed dislocations emitted from grain boundaries, those dislocations interacting with intragranular dislocations and the formation of dislocation cells in the grains. Based on those experimental results, the low-temperature creep mechanisms in pure aluminum at ε̇ < 10-10 s-l have been discussed. © 2011 The Japan Institute of Metals.

    DOI: 10.2320/matertrans.M2010405

  • コイルばねクリープ試験法による改良9Cr‐1Mo鋼の極低速クリープ挙動評価

    山崎重人, 光原昌寿, 池田賢一, 波多聰, 中島英治

    材料とプロセス(CD-ROM)   23 ( 2 )   ROMBUNNO.277   2010年9月

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    記述言語:日本語  

    コイルばねクリープ試験法による改良9Cr‐1Mo鋼の極低速クリープ挙動評価

  • Pt系分散強化合金の低応力領域でのクリープ特性の検討

    富田成明, 浜島和雄, 山崎重人, 光原昌寿, 池田賢一, 波多聰, 中島英治

    日本金属学会講演概要   146th   365   2010年3月

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    記述言語:日本語  

    Pt系分散強化合金の低応力領域でのクリープ特性の検討

  • コイルばねクリープ試験法による高Cr鋼の低速クリープ挙動評価

    山崎重人, 藤本健資, 光原昌寿, 池田賢一, 波多聰, 中島英治, 木村光男

    材料とプロセス(CD-ROM)   22 ( 2 )   ROMBUNNO.PS-35   2009年9月

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    記述言語:日本語  

    コイルばねクリープ試験法による高Cr鋼の低速クリープ挙動評価

  • コイルばねクリープ試験法によるSUS304鋼のクリープ挙動解析

    光原昌寿, 山崎重人, 池田賢一, 波多聰, 中島英治

    材料とプロセス(CD-ROM)   21 ( 2 )   ROMBUNNO.TO121   2008年9月

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    記述言語:日本語  

    コイルばねクリープ試験法によるSUS304鋼のクリープ挙動解析

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講演・口頭発表等

  • 加速クリープに関するレビュー ~加速クリープに関する現状の理解と問題点~

    山﨑重人

    日本鉄鋼協会「高温材料の高強度化」研究会 第6回研究会  2021年4月 

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    開催年月日: 2021年5月

    記述言語:日本語  

    国名:日本国  

  • ミルフィーユ構造Mg系合金に生じるキンクバンドの特徴

    山﨑重人

    日本鉄鋼協会 材料の組織と特性部会 若手フォーラム 第3 回研究会  2020年11月 

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    開催年月日: 2021年5月

    記述言語:日本語  

    国名:日本国  

  • 長周期積層構造 Mg-Zn-Y 合金におけるキンク形成過程

    山﨑重人, 徳澄翼, 光原昌寿, 中島英治, 田中將己

    第62回日本顕微鏡学会九州支部学術講演会  2020年11月 

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    開催年月日: 2021年5月

    記述言語:日本語  

    国名:日本国  

  • コバルト添加フェライト系耐熱鋼のクリープ強度と磁気特性の関係

    山﨑重人

    日本鉄鋼協会 第181回春季講演大会  2021年3月 

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    開催年月日: 2021年5月

    記述言語:日本語  

    国名:日本国  

  • LPSO単相Mg-Zn-Y合金におけるキンク変形の前駆現象

    光原昌寿、山﨑重人、惣島雅樹、中島英治、萩原幸司、藤居俊之

    日本金属学会2019年秋期(第165回)講演大会  2019年9月 

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    開催地:岡山大学  

  • 定負荷速度引張試験により測定した2元系アルミニウム固溶体合金のセレーション挙動

    古賀鈴, 山﨑重人, 光原昌寿, 中島英治, 秋吉竜太郎, 徳田健二, 有賀康博

    軽金属学会 第134 回春期大会  2018年5月 

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    開催地:熊本大学  

  • 耐熱合金のクリープ変形の測定と定量的組織観察

    山﨑重人

    日本金属学会 第1回若手研究グループ研究会「多様な先端観察・測定法を用いた組織の定量と力学特性解析への適用」  2018年4月 

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    開催地:弘前大学  

  • レーザー積層法により作製した耐熱アルミニウム合金への遷移元素添加

    奥平有, 山﨑重人,光原昌寿,中島英治,西田稔, 楠井潤, 安達充

    日本金属学会 春期(第162回)講演大会  2018年3月 

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    開催地:千葉工業大学  

  • 電子ビーム積層法およびレーザー積層法により作製したAC8A合金の高温強度特性

    奥平有, 山﨑重人,光原昌寿,中島英治,西田稔, 楠井潤, 安達充

    日本金属学会 春期(第162回)講演大会  2018年3月 

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    開催地:千葉工業大学  

  • Relationship between Creep Deformation and Microstructure of Heat-Resistant Alloys 招待 国際会議

    S. Yamasaki

    MJIIT MICROSCOPY LABORATORY WORKSHOP SERIES-2  2018年3月 

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    開催地:マレーシア工科大学   国名:マレーシア  

  • 長時間時効した“Hastelloy X”合金の組織とクリープ変形挙動(第二報)

    山﨑重人, 光原昌寿, 中島英治, 齊藤大蔵, 吉岡洋明

    平成29年度 3月期 耐熱金属材料第123委員会  2018年3月 

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    開催地:東京工業大学  

  • マイクロシェブロンノッチ曲げ試験法とSEM/FIBトモグラフィーを組み合わせた亀裂進展経路の3次元解析

    吉田歩夢, 本田佳暉, 山﨑重人, 光原昌寿, 中島英治, 後藤裕明, 津田圭一

    第59回 日本顕微鏡学会 九州支部集会・学術講演会  2017年12月 

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    開催地:ニューウェルシティ宮崎  

  • 窒素添加マルテンサイト耐熱鋼のクリープ変形挙動

    山﨑重人, 當山守人, 堀翔太郎, 光原昌寿, 中島英治

    高温変形の組織ダイナミクス研究会「平成29年度夏の学校」  2017年9月 

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    開催地:サンヒルズ三河湾  

  • 多結晶Ni基耐熱合金のクリープ変形中に生じる転位とγ'析出物の相互作用

    百武優佑, 山﨑重人, 光原昌寿, 中島英治

    高温変形の組織ダイナミクス研究会「平成29年度夏の学校」  2017年9月 

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    開催地:サンヒルズ三河湾  

  • 定負荷速度引張試験により測定したAl合金とNi合金のセレーション挙動

    古賀鈴, 山﨑重人, 光原昌寿, 中島英治, 秋吉竜太郎, 高木康夫 徳田健二

    高温変形の組織ダイナミクス研究会「平成29年度夏の学校」  2017年9月 

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    開催地:サンヒルズ三河湾  

  • WC-Co 超硬合金の残留応力解析

    本田佳暉, 山﨑重人, 光原昌寿, 中島英治, 後藤裕明, 津田圭一

    日本金属学会 秋期(第161回)講演大会  2017年9月 

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    開催地:北海道大学  

  • Al 添加α-Ti 合金における双晶界面の高分解能観察

    徳永隼人, 山﨑重人, 光原昌寿, 中島英治, 塚本元気, 國枝知徳

    日本金属学会 秋期(第161回)講演大会  2017年9月 

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    開催地:北海道大学  

  • 金属積層工法を用いたAC8A アルミニウム合金の高温強度特性

    奥平有, 山﨑重人, 光原昌寿, 中島英治, 西田稔, 安達充, 栗田健也, 永田佳彦, 小岩井修二

    日本金属学会 秋期(第161回)講演大会  2017年9月 

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    開催地:北海道大学  

  • Laves相により強化されたフェライト単相耐熱鋼のクリープ変形挙動と微細組織

    堀翔太郎, 山﨑重人, 光原昌寿, 中島英治, 木村一弘

    日本鉄鋼協会 第174 回秋季講演大会  2017年9月 

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    開催地:北海道大学  

  • Development of new ferritic heat-resistant steel with high nitrogen and tungsten addition 国際会議

    S. Yamasaki, M. Mitsuhara and H. Nakashima

    IU-MRS (International union of Materials Research Society) 2017  2017年8月 

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    開催地:京都大学   国名:日本国  

  • 長時間時効したHastelloy X合金の組織とクリープ変形挙動

    山﨑重人, 光原昌寿, 中島英治, 齊藤大蔵, 吉岡洋明

    平成29年度 7月期 耐熱金属材料第123委員会  2017年7月 

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    開催地:東京工業大学  

  • 窒素含有マルテンサイト鋼のクリープ変形挙動

    山﨑重人、今村祐輔、光原昌寿、中島英治

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 平成29年度 合同学術講演大会  2017年6月 

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    開催地:熊本大学  

  • チタンの双晶発生に及ぼす固溶元素の影響

    徳永隼人, 山﨑重人, 光原昌寿, 中島英治, 塚本元気, 國枝知徳

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 平成29年度 合同学術講演大会  2017年6月 

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    開催地:熊本大学  

  • HPT加工をした純鉄の摩擦特性と微細組織

    岩﨑眞澄, 山﨑重人, 光原昌寿, 中島英治, 西田稔, 堀井基弘, 戸高義一

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 平成29年度 合同学術講演大会  2017年6月 

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    開催地:熊本大学  

  • ラスマルテンサイト鋼のクリープ変形挙動に及ぼす転位密度の影響

    當山守人, 山﨑重人, 光原昌寿, 中島英治

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 平成30年度 合同学術講演大会  2018年6月 

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    開催地:北九州国際会議場  

  • 高ひずみ分解能単軸クリープ試験による極低ひずみ速度変形挙動の評価

    加藤 由輝, 山﨑重人, 光原昌寿, 中島英治

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 平成30年度 合同学術講演大会  2018年6月 

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    開催地:北九州国際会議場  

  • Creep Deformation and Strengthening Mechanism in Newly Developed Ni-20Cr-15Co-1Ti-2Al-8W Polycrystalline HeatResistant Alloy 招待 国際会議

    M. Mitsuhara, T. Ito, S. Yamasaki, H. Nakashima, M. Nishida, M. Yonemura

    18th International Conference on the Strength of Materials  2018年6月 

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    開催地:オハイオ州立大  

  • 耐熱合金の微細組織の観察・測定と評価

    山﨑重人

    IHI Materials Forum 2018  2018年8月 

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    開催地:IHI 横浜事業所  

  • フェライト系耐熱鋼のクリープ強度に及ぼす W と Co 添加の影響

    山﨑重人, 光原昌寿, 中島英治

    高温変形の組織ダイナミクス研究会「平成 30 年度 夏の学校」  2018年9月 

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    開催地:ホテル春慶屋  

  • 2 元系アルミニウム固溶体合金のセレーシ ョン挙動

    古賀鈴, 山﨑重人, 光原昌寿, 中島英治, 秋吉竜太郎, 木村申平

    高温変形の組織ダイナミクス研究会「平成 30 年度 夏の学校」  2018年9月 

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    開催地:ホテル春慶屋  

  • 金属表面に形成する潤滑油膜に対する結晶方位と結晶粒径の影響

    岩﨑眞澄, 山﨑重人, 光原昌寿, 中島英治, 西田稔, 殿塚一希

    日本鉄鋼協会 第176回秋季講演大会  2018年9月 

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    開催地:東北大学  

  • 焼きならし処理のみを施したGr.91鋼における静的時効中のM23C6炭化物成長挙動

    荒金遼河, 山﨑重人, 光原昌寿, 中島英治, 澤田浩太, 木村一弘

    日本鉄鋼協会 第176回秋季講演大会  2018年9月 

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    開催地:東北大学  

  • 高Crフェライト系耐熱鋼溶接熱影響部再現組織への前焼き戻し処理の影響

    佐々木王城, 山﨑重人, 光原昌寿, 中島英治, 澤田浩太,久布白圭司

    日本鉄鋼協会 第176回秋季講演大会  2018年9月 

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    開催地:東北大学  

  • ラスマルテンサイト鋼のクリープ変形挙動に与える転位密度の影響

    當山守人, 山﨑重人, 光原昌寿, 中島英治

    日本鉄鋼協会 第176回秋季講演大会  2018年9月 

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    開催地:東北大学  

  • 高温変形の未踏領域 ~及川洪先生「単相金属・合金の高温クリープ挙動: その理解と問題点」のレビューに基づいて~

    山﨑重人

    鉄鋼協会「高温材料の高強度化」研究会 第2回研究会  2018年10月 

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    開催地:淡路 ゆうなぎ荘  

  • Al-Mg-Si合金とAl-Mg-Zn合金のセレーション挙動

    三池友樹, 山﨑重人, 光原昌寿, 中島英治

    軽金属学会 第136回春期大会  2019年5月 

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    開催地:富山国際会議場  

  • デジタル画像相関法による純鉛の局所クリープ変形挙動解析

    奥村啓太, 山﨑重人, 光原昌寿, 中島英治

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 令和元年度 合同学術講演大会  2019年6月 

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    開催地:熊本県民交流館パレア  

  • フェライト系耐熱鋼の磁気変態点変化がクリープ変形に及ぼす影響

    藤野翔太, 山﨑重人, 光原昌寿, 中島英治

    日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部 共催 令和元年度 合同学術講演大会  2019年6月 

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    開催地:熊本県民交流館パレア  

  • In-situ EBSD characterization of deformation behavior of primary alpha phase in Ti-6Al-4V 国際会議

    W. Li, S. Yamasaki, M. Mitsuhara, H. Nakashima

    The 14th World Conference on Titanium  2019年6月 

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    開催地:Nantes, France  

  • 耐熱合金の高温変形 招待

    山﨑重人

    駒場材料学セミナー  2019年8月 

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    開催地:東京大学 駒場キャンパス  

  • 定負荷速度引張試験で測定したアルミニウム合金のセレーション変形

    山﨑重人, 三池友樹, 光原昌寿, 中島英治, 秋吉竜太郎, 木村申平

    高温変形の組織ダイナミクス研究会「2019年度 夏の学校」  2019年9月 

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    開催地:石川県青少年総合研修センター  

  • フェライト系耐熱鋼の実用ひずみ速度域でのクリープ変形

    山﨑重人, 光原昌寿, 中島英治

    日本鉄鋼協会  2019年9月 

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    開催地:岡山大学  

  • Creep behavior of ferritic heat resistant steel added with nitrogen 国際会議

    S. Yamasaki, M. Mitsuhara and H. Nakashima

    Joint EPRI-123HiMAT International Conference on Advances in High Temperature Materials  2019年10月 

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    開催地:Nagasaki Brick Hall  

  • クリープ試験の改良と応用 招待

    山﨑重人, 光原昌寿, 中島英治

    日本鉄鋼協会「高温材料の高強度化」研究会  2019年11月 

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    開催地:レクトーレ箱根強羅  

  • LPSO単相多結晶Mg-Zn-Y合金におけるキンク形成過程

    山﨑重人, 徳澄翼, 光原昌寿, 中島英治, 萩原幸司, 藤居俊之

    軽金属学会 第137回秋期講演大会  2019年11月 

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    開催地:東京農工大学 小金井キャンパス  

  • Ti-6Al-4V合金の室温クリープ変形挙動の評価

    出口岬,山﨑重人,光原昌寿, 中島英治, 大田祐太朗

    軽金属学会 第137回秋期講演大会  2019年11月 

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    開催地:東京農工大学 小金井キャンパス  

  • Growth behavior of M23C6 carbides in high-Cr ferritic heat-resistant steels 国際会議

    M. Mitsuhara, S. Yamasaki, R. Arakane, R. Takao, H. Nakashima

    Joint EPRI-123HiMAT International Conference on Advances in High Temperature Materials  2019年10月 

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    開催地:Nagasaki Brick Hall  

  • Microscopic observation of formation process of kink bands in Mg-Zn-Y alloy with LPSO phase 招待 国際会議

    Masatoshi Mitsuhara, Shigeto Yamasaki, Hideharu Nakashima, Koji Hagihara, Toshiyuki Fujii

    Mini-symposium: ”Elastic defects and structures. Modeling and experiments”  2019年8月 

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    開催地:Kyushu University  

  • αTiにおけるすべり系活動への結晶粒間相互作用の影響とその範囲

    河野義樹、眞山剛、光原昌寿、山﨑重人、佐藤満弘

    日本金属学会2019年秋期(第165回)講演大会  2019年9月 

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    開催地:岡山大学  

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MISC

  • レーザ積層造形法と電子ビーム積層造形法で作製したAC8Aアルミニウム合金のミクロ組織と引張特性—Microstructure and tensile strength of AC8A aluminum alloy fabricated by laser-based powder bed fusion and electron-based powder bed fusion—特集 軽金属材料の三次元造形技術

    安達 充, 奥平 有, 山﨑 重人, 光原 昌寿, 中島 英治, 小岩井 修二, 橋詰 良樹, 村上 勇夫, 寺田 大将

    軽金属   2022年5月

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    記述言語:日本語  

  • Ti-6Al-4V合金における室温クリープ中の転位の運動様式と変形組織の発達過程

    出口 岬, 山﨑 重人, 光原 昌寿, 中島 英治, 大田 祐太朗

    チタン = Titanium Japan   2021年10月

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    記述言語:日本語  

    Dislocation Motion and Microstructure Evolution Deformed during Creep at Room Temperature in Ti-6Al-4V Alloy

産業財産権

特許権   出願件数: 2件   登録件数: 0件
実用新案権   出願件数: 0件   登録件数: 0件
意匠権   出願件数: 0件   登録件数: 0件
商標権   出願件数: 0件   登録件数: 0件

所属学協会

  • 軽金属学会

  • 日本鉄鋼協会

  • 日本鉄鋼協会

  • 日本金属学会

  • 軽金属学会

  • 日本金属学会

▼全件表示

学術貢献活動

  • 2023-2024年度講演大会委員

    日本金属学会  ( Japan ) 2023年5月

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    種別:大会・シンポジウム等 

  • 学術論文等の審査

    役割:査読

    2022年

     詳細を見る

    種別:査読等 

    外国語雑誌 査読論文数:3

    日本語雑誌 査読論文数:3

  • ISIJ international 国際学術貢献

    2021年6月 - 2025年3月

     詳細を見る

    種別:学会・研究会等 

  • 鉄と鋼

    2021年6月 - 2025年2月

     詳細を見る

    種別:学会・研究会等 

  • 座長

    軽金属学会 第140回春期大会  ( Japan ) 2021年5月

     詳細を見る

    種別:大会・シンポジウム等 

  • 学術論文等の審査

    役割:査読

    2021年

     詳細を見る

    種別:査読等 

    外国語雑誌 査読論文数:6

    日本語雑誌 査読論文数:2

  • 学術論文等の審査

    役割:査読

    2020年

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    種別:査読等 

    外国語雑誌 査読論文数:4

  • 学術論文等の審査

    役割:査読

    2019年

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    種別:査読等 

    外国語雑誌 査読論文数:3

  • 座長

    日本金属学会 春期(第162回)講演大会  ( 千葉工業大学 ) 2018年3月

     詳細を見る

    種別:大会・シンポジウム等 

  • 学術論文等の審査

    役割:査読

    2018年

     詳細を見る

    種別:査読等 

    外国語雑誌 査読論文数:2

    日本語雑誌 査読論文数:1

    国際会議録 査読論文数:0

    国内会議録 査読論文数:0

  • 座長 国際学術貢献

    IU-MRS (International union of Materials Research Society) 2017  ( 京都大学 ) 2017年8月

     詳細を見る

    種別:大会・シンポジウム等 

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共同研究・競争的資金等の研究課題

  • マルテンサイト鋼の実用環境におけるクリープ変形機構の解明

    2023年 - 2024年

    日本鉄鋼協会 鉄鋼研究振興助成

      詳細を見る

    担当区分:研究代表者  資金種別:受託研究

  • 微小片持ちはり試験片を用いた転位間相互作用の測定

    研究課題/領域番号:22H01813  2022年 - 2024年

    日本学術振興会  科学研究費助成事業  基盤研究(C)

      詳細を見る

    資金種別:科研費

  • 菊池バンド幅解析と画像相関法を併用した任意のミクロ領域からの応力-ひずみ曲線取得

    2021年 - 2022年

    日本金属学会フロンティア研究助成

      詳細を見る

    担当区分:研究代表者  資金種別:受託研究

  • 第2回日本金属学会フロンティア研究助成

    2021年

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    資金種別:寄附金

  • 磁気変態に伴う拡散速度変化に着目した耐熱鋼の新しいクリープ強化概念の確立

    研究課題/領域番号:19K15277  2019年 - 2020年

    日本学術振興会  科学研究費助成事業  基盤研究(C)

      詳細を見る

    資金種別:科研費

  • 磁気変態に伴う拡散速度変化に着目した耐熱鋼の新しいクリープ強化概念の確立

    研究課題/領域番号:19K15277  2019年 - 2020年

    日本学術振興会  科学研究費助成事業  若手研究

      詳細を見る

    担当区分:研究代表者  資金種別:科研費

  • Ti合金の室温クリープに関する研究

    2018年5月 - 2020年3月

    共同研究

      詳細を見る

    担当区分:研究代表者  資金種別:その他産学連携による資金

  • 高温における亜粒界強化機構の解明

    研究課題/領域番号:18H01739  2018年 - 2020年

    日本学術振興会  科学研究費助成事業  基盤研究(C)

      詳細を見る

    資金種別:科研費

  • 高温における亜粒界強化機構の解明

    研究課題/領域番号:18H01739  2018年 - 2020年

    日本学術振興会  科学研究費助成事業  基盤研究(B)

      詳細を見る

    担当区分:研究分担者  資金種別:科研費

  • アルミニウム合金のしきい応力以下での極低速クリープ変形機構

    2018年 - 2019年

    平成30年度アルミニウム研究助成事業

      詳細を見る

    担当区分:研究代表者  資金種別:受託研究

  • 分散強化鋼の分散状態の不均一性がしきい応力に及ぼす影響

    2017年6月 - 2018年3月

    共同研究

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    担当区分:研究代表者  資金種別:その他産学連携による資金

  • ECCI法によるHCP材料の転位観察

    2017年6月 - 2018年3月

    共同研究

      詳細を見る

    担当区分:研究代表者  資金種別:その他産学連携による資金

  • 多結晶金属中の転位組織の不均一性とその力学特性への影響

    研究課題/領域番号:17H06933  2017年 - 2018年

    日本学術振興会  科学研究費助成事業  基盤研究(C)

      詳細を見る

    資金種別:科研費

  • 多結晶金属中の転位組織の不均一性とその力学特性への影響

    研究課題/領域番号:17H06933  2017年 - 2018年

    科学研究費助成事業  若手研究(スタートアップ)

      詳細を見る

    担当区分:研究代表者  資金種別:科研費

▼全件表示

教育活動概要

  • 工学府材料工学専攻および工学部材料工学科における下記担当授業科目の担当ならびに所属研究室での研究指導を行っている。

担当授業科目

  • 結晶化学

    2023年12月 - 2024年2月   冬学期

  • 自動車用金属材料学

    2023年12月 - 2024年2月   冬学期

  • 結晶塑性学

    2023年12月 - 2024年2月   冬学期

  • 耐熱材料工学

    2023年12月 - 2024年2月   冬学期

  • 回折結晶学

    2023年12月 - 2024年2月   冬学期

  • 高温材料強度学第一

    2023年10月 - 2023年12月   秋学期

  • 無機材料解析学

    2023年10月 - 2023年12月   秋学期

  • 無機材料解析学

    2023年10月 - 2023年12月   秋学期

  • 高温材料強度学

    2023年10月 - 2023年12月   秋学期

  • 自動車用金属材料学

    2022年12月 - 2023年2月   冬学期

  • 高温材料強度学第二

    2022年12月 - 2023年2月   冬学期

  • 耐熱材料工学

    2022年12月 - 2023年2月   冬学期

  • 結晶塑性学

    2022年12月 - 2023年2月   冬学期

  • 非鉄材料工学

    2022年10月 - 2023年3月   後期

  • 結晶塑性学

    2021年12月 - 2022年2月   冬学期

  • 高温材料強度学第二

    2021年10月 - 2021年12月   秋学期

  • 非鉄構造材料工学

    2021年10月 - 2021年12月   秋学期

  • 非鉄材料工学

    2021年10月 - 2021年12月   秋学期

  • 物質プロセス工学演習第二C

    2021年4月 - 2022年3月   通年

  • 結晶塑性学

    2021年4月 - 2021年9月   前期

  • 物質プロセス工学演習第二C

    2020年4月 - 2021年3月   通年

  • 物質科学情報集約演習

    2020年4月 - 2021年3月   通年

▼全件表示

その他教育活動及び特記事項

  • 2021年  クラス担任  学部

  • 2021年  その他特記事項  九州大学未来創成科学者育成プロジェクト

     詳細を見る

    九州大学未来創成科学者育成プロジェクト

学内運営に関わる各種委員・役職等

  • 2022年4月 - 2023年3月   部門 安全衛生委員会委員