九州大学 研究者情報
発表一覧
金子 賢治(かねこ けんじ) データ更新日:2024.02.22

教授 /  工学研究院 材料工学部門 材料加工工学


学会発表等
1. 齋藤 晃, 津田 健治, 田中 通義, 金子 賢治, 蔡 安邦, 7p-R-8 HAADF法によるデカゴナル準結晶の観察II, 日本物理学会講演概要集, 1997.09.
2. 齋藤 晃, 津田 健治, 田中 通義, 金子 賢治, 蔡 安邦, 7p-R-7 HAADF法によるデカゴナル準結晶の観察, 日本物理学会講演概要集, 1997.09.
3. 大東 琢治, 金子 賢治, 杉山 昌章, 田中 信夫, 土谷 浩一, 廣澤 渉一, 宝野 和博, 松原 英一郎, 松村 晶, 村田 薫, 戸田 裕之, 特集「顕微鏡法による材料開発のための微細構造研究最前線(7)-3D/4Dイメージング-」特集企画にあたって, まてりあ : 日本金属学会会報, 2007.12.
4. 金子 賢治, EDSの基礎, 日本顕微鏡学会 分析電子顕微鏡討論会, 2015.09.
5. 金子 賢治, EDSの基礎, 第32回分析電子顕微鏡討論会, 2016.09.
6. Kenji Kaneko, Three-dimensional characterization of various crystalline materials by electron microscopy, AMTC5, 2016.05, [URL], Nanoscale characterization plays a vital role in process, design and property of materials used in nanoscience and nanotechnology. Large numbers of papers have been published concerning nanoscale materials based on characterizations by electron microscopes displaying 2D images, which is not reflecting the true 3D morphologies or dispersions of the materials precisely, and authors had to correlate those 2D results with 3D physical properties of materials. Therefore, it is extremely important to learn the correlation between the 3D physical properties of materials and their sizes, structures, compositions, dispersions and morphologies. Recent development of fully-digitized and automated electron microscopes, both scanning electron microscope (SEM) and transmission electron microscope (TEM), as well as advancement of fast computers and commercial software let us achieve 3D information by electron microscopes. A 3D object can be reconstructed from a series of 2D images obtained from electron microscopes, either the combination of focus ion beam (FIB) and SEM via slice-sectioning (SS) or that of TEM and computed tomography (CT), to determine dispersion and morphology of the object in the order of nanometer.
In this talk, I will present recent results obtained from various crystalline materials obtained by TEM-CT and FIB-SEM-SS..
7. 金子 賢治, FIB-SEMによる鉄鋼材料の3次元解析, 日本顕微鏡学会, 2015.12.
8. 金子 賢治, EDSの基礎, 日本顕微鏡学会 分析電子顕微鏡討論会, 2015.09.
9. 金子 賢治, EDSの基礎, 第31回分析電子顕微鏡討論会, 2015.09.
10. Kenji Kaneko, Three-dimensional characterization of various crystalline materials by electron microscopy Two dee or not two dee, that is the question!, NIMS Conference 2015, 2015.07, [URL], Nanoscale characterization plays a vital role in process, design and property of materials used in nanoscience and nanotechnology. Large numbers of papers have been published concerning nanoscale materials based on characterizations by electron microscopes displaying 2D images, which is not reflecting the true 3D morphologies or dispersions of the materials precisely, and authors had to correlate those 2D results with 3D physical properties of materials. Therefore, it is extremely important to learn the correlation between the 3D physical properties of materials and their sizes, structures, compositions, dispersions and morphologies. Recent development of fully-digitized and automated electron microscopes, both scanning electron microscope (SEM) and transmission electron microscope (TEM), as well as advancement of fast computers and commercial software let us achieve 3D information by electron microscopes. A 3D object can be reconstructed from a series of 2D images obtained from electron microscopes, either the combination of focus ion beam (FIB) and SEM via slice-sectioning (SS) or that of TEM and computed tomography (CT), to determine dispersion and morphology of the object in the order of nanometer.
In this talk, I will present recent results obtained from various crystalline materials obtained by TEM-CT and FIB-SEM-SS..
11. 金子 賢治, 河野 理香, 山田和広, 菊池 正夫, 原 徹, SUS347における粒界析出物の3次元ナノ解析, 日本鉄鋼協会第169回春季講演大会, 2015.03.
12. 金子 賢治, Three-dimensional nanostructural analysis of artificial pinning in coated conductors by electron tomography, The 15th IUMRS-International Conference in Asia (IUMRS-ICA 2014), 2014.09, [URL], In high temperature superconductors, artificial pinning centers (APCs) are intentionally introduced to pin the vortices effectively for compensation of the intrinsic field angle anisotropy and to improve Jc characteristics. APCs have been analyzed via various microscopic methods in detail, many of them are actually in 2D, which does not represent 3D nature of APCs. The nanostructural characterization of APCs in 3D (distribution, morphology, volume, etc.) are of worthwhile for further understanding and improvement of the superconducting properties, and hence for designing of future high temperature superconductors. Electron tomography, a combination of transmission electron microscopy and computed tomography, was therefore applied on APCs to acquire 3D information of them at nanoscale resolution. During my presentation, both three-dimensional electron tomography and actual application of it on artificial pinning centers in various dimension, will be presented..
13. 金子 賢治, 透過型電子顕微鏡を用いた3D/4D観察の現状, 日本鉄鋼協会第167回春季講演大会, 2014.03.
14. 金子 賢治, Three-Dimensional Electron Tomography for Materials Science and Engineering, The 14th IUMRS-International Conference in Asia (IUMRS-ICA 2013), 2013.12, [URL], Currently, there are several “tomographic” methods available to acquire three-dimensional information of materials, and have been applied for various types of materials; three-dimensional atomic probe at atomic resolution, electron tomography via focused ion beam (FIB) method at submicron resolution, and electron tomography via (scanning) transmission electron microscopes, (S)TEM, at a few nanometer resolution. Three-dimensional electron tomography (3D-ET), a technique originally established in the field of life sciences, has been developed and applied for materials science and engineering, which is a useful technique for reconstructing an object from a series of projections acquired by a (S)TEM. In addition, every materials available in the world is actually in 3D and their properties are usually dealt in 3D, so that characterization of materials should also be dealt in 3D at micro- and nano-scale. Recent progress of fully-digitized and automated (S)TEM let us achieve 3D characterization for not only to determine the size and distribution of objects but also to provide information about the 3D morphology.
Five different types of information was achieved by 3D-ET: the morphological information of metallic nanoparticles decorated by supramolecules, the distribution of metallic nanoparticles within catalyst, the crystal habit of CeO2 for catalytic activities, the morphological transformation of GP zones due to plastic deformation, and morphology of precipitates within Al alloy.
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15. 金子 賢治, 界面の微構造解析, 第128回講演大会(福岡工業大学), 2013.09, [URL].
16. Kenji Kaneko, Electron Tomography for Materials Science and Engineering, International Conference on Electron Microscopy and XXXIV Annual Meeting of the Electron Microscope Society of India, 2013.07, [URL].
17. 金子 賢治, 電子線トモグラフィ、TEMとFIB, 平成24年度「マテリアル電子線トモグラフィ研究部会」講演会, 2013.03.
18. 金子 賢治, 材料と電子顕微鏡, 第4回レーザー学会「レーザーバイオ医療」技術専門委員会, 2013.03.
19. Hadi Razavi Khosroshahi, Xin Liu, Noritaka Saito, Kunihiko Nakashima, Kenji Kaneko, Effect of nano-sized particles on the mechanical properties of Y2O3, 8th International Forum on Advanced Materials Science and Technology, IFAMST 2012, Two types of TiO2/Y2O3 and ZrO2/Y2O3 composites were fabricated for enhancing the mechanical properties of Y2O3 ceramic. Results showed that ZrO2/Y2O3 composite dramatically increased the strength and toughness as 417 MPa and 4.4 MPa.m1/2, respectively..
20. T. Nishiyama, K. Yamada, Ryo Teranishi, Kenji Kaneko, T. Kato, T. Izumi, Y. Shiohara, Three-dimensional characterization of BaZrO3 precipitates in Y1-xGdxBa2Cu3O7-y prepared by TFA-MOD using STEM-tomography, 8th International Forum on Advanced Materials Science and Technology, IFAMST 2012, Y1-xGdxBa2Cu3O7-y film with BaZrO3 was fabricated on CeO2 buffered LaMnO3/ion beam assisted deposition MgO/Gd2Zr2O7/Hastelloy C276TM substrates by the trifluoroacetates metal organic deposition process, whose microstructural and elemental analyses were performed by transmission electron microscopy. Y1-xGdxBa2Cu3O7-y film with the thickness about 700 nm was found composed of c-axis oriented grains and large numbers of randomly oriented precipitates, such as (Y,Gd)2Cu2O5, CuO and BaZrO3. (Y,Gd)2Cu2O5 and CuO precipitates were heterogeneously dispersed in the Y1-xGdxBa2Cu3O7-y matrix with their sizes ranging between 100 and 200 nm, and BaZrO3 precipitates were uniformly dispersed with their sizes ranging between 10 and 20 nm. Electron tomography with elemental information was performed further to reveal the threedimensional information of BaZrO3 precipitates..
21. T. Nishiyama, K. Kaneko, K. Yamada, R. Teranishi, T. Kato, T. Hirayama, H. Tobita, T. Izumi, Y. Shiohara, Three-dimensional analysis of BaHfO3 precipitates in GdBa2Cu3Oy via scanning transmission electron tomography, ISS2012, 2012.12, [URL].
22. K. Yamada, K. Kaneko, Y. Tachibanaki, T. Nishiyama, R. Teranishi, M. Itoh, O. Miura, R. Kita, INFLUENCES OF CRYSTALLIZATION CONDITIONS ON THE GROWTH OF GdBa2Cu3Oy FILMS FABRICATED BY FLUORINE-FREE MOD METHOD, ISS2012, 2012.12, [URL].
23. K. Kaneko, T. Nishiyama, K. Yamada, R. Teranishi, T. Kato, Y. Yamada, T. Izumi and Y. Shiohara, Three-dimensional characterization of artificial pinning centers in high temperature superconductors by three-dimensional electron tomography, ISS2012, 2012.12, [URL].
24. K. Konya, K. Ootaguro, T. Nishiyama, R. Teranishi, T. Kiss, K. Yamada, K. Kaneko, M. Yoshizumi, T. Izumi , Effect of holding temperature on microstructures and Jc properties of YBa2Cu3O7-X films fabricated by TFA-MOD method, ISS2012, 2012.12.
25. T. Watanabe, T. Kamata, T. Maebatake, R. Teranishi, T. Kiss, K. Yamada, K. Kaneko, M. Yoshizumi, T. Izumi, Study of factors in joint resistance for GdBCO coated conductors, ISS2012, 2012.12, Joint techniques are important to manufacture long superconducting tapes for industrial applications, such as superconducting power cables and wires. It has been reported that GdBa2Cu3Oy (GdBCO) coated conductors have higher critical current and critical temperature than YBCO, so that the development of GdBCO coated conductor has been investigated. However, it was reported that the joint resistance of GdBCO was found higher than that of YBCO even the same Ag diffusion joint process were applied. In this paper, the elemental distribution maps at joint part of the coated conductors were investigated to examine the cause of joint resistance. Scanning transmission electron microscopy (STEM) and energy-dispersive X-ray spectroscopy (EDS) analysis of GdBCO tape showed the reduction of oxygen in GdBCO layer at Ag/GdBCO interface region. This oxygen reduction in GdBCO layer may cause degradation of superconducting properties and increase of interfacial resistance between GdBCO and Ag, that may have lead the higher joint resistance in Ag/GdBCO coated conductor than that of Ag/YBCO one..
26. J. S. Barnard, J. H. Sharp, Satoshi Hata, Masatoshi Mitsuhara, Kenji Kaneko, K. Higashida, 3-dimensional imaging of dislocation microstructures by electron beams, 2011 MRS Fall Meeting, 2012.12, We review the progress in the electron tomography of dislocation microstructures in the transmission electron microscope (TEM). Dislocation contrast is visible both in conventional TEM and scanning TEM (STEM) modes and, despite the complicated intensity variations, dislocation contrast can be isolated using computational filtering techniques prior to reconstruction. We find that STEM annular dark-field (STEM-ADF) imaging offers significant advantages in terms of dislocation contrast and background artifacts. We present several examples, both in semiconducting and metallic systems, illustrating the properties of 3D dislocations. We present the high-angle triple-axis (HATA) specimen holder where the diffraction condition can be chosen at will and dislocation tomograms of multiple reflections can be combined. 3D dislocations are analyzed in terms of dislocation density and dislocation nodal structures. Several avenues of study are suggested that may exploit the 3D dislocation data..
27. 山田和広, 金子賢治, 谷口 慎, 完山正林, 岩堀安晃, 鈴木直久, アルミニウム合金における析出物のFIBトモグラフィ法による解析, 第28回 分析電子顕微鏡討論会, 2012.09, [URL].
28. 金子 賢治, GdBa2Cu3O7-xにおけるBaHfO3のSTEMトモグラフィ法による解析, 第28回 分析電子顕微鏡討論会, 2012.09, [URL].
29. 金子賢治, TEM-CT法とFIB-シリアルセクショニング法, 第28回 分析電子顕微鏡討論会, 2012.09, [URL].
30. 山田和広, 金子賢治, 完山正林, 鈴木直久, シリアルセクショニング法によるAl合金中析出物の3次元可視化, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
31. Hadi Razavi Khosroshahi, 大串将巧, 齋藤敬高, 中島邦彦, 金子賢治, Y2O3基複合材料の作製および機械的特性, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
32. 佐藤直子, 足立吉隆, 金子賢治, ボイドと組織の三次元解析によるDP鋼の破壊挙動の検討, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
33. 西山武志, 山田和広, 金子賢治, 加藤丈晴, 飛田浩史, 和泉輝郎, 塩原 融, GdBa2Cu3O7-x厚膜中におけるBaHfO3の電子線トモグラフィによる解析, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
34. 權堂貴志, 金子賢治, 伊田進太郎, 石原達己, SBA-15細孔構造へのTiO2添加量が及ぼす影響, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
35. 竹田恵一, 金子賢治, 北山幹人, 大尾岳史, 窒化珪素における粒界相界面の希土類イオン偏析現象の解明, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
36. 福永達也, 金子賢治, 中田伸生, 菊池正夫, TEM内でのその場加熱による鋭敏化処理と微視的構造解析, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
37. 和田勇希, 小林知世, 山田和広, 金子賢治, 池田賢一, 中島英治, 菊池正夫, 高田健, 佐賀誠, 潮田浩作, Al-Mg-Si系合金過時効材の超高圧電子顕微鏡によるその場引張試験, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
38. 井上剣太, 菊山達彦, 寺西亮, 宗藤伸治, 金子賢治, パルスレーザー蒸着法によるGdBa2Cu3Oy超伝導薄膜の結晶配向への影響因子, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
39. 大串将巧, Hadi Razavi Khosroshahi, 池田拓之, 齋藤敬高, 中島邦彦, 金子賢治, 酸化イットリウム焼結体強度に炭化ケイ素分散が及ぼす影響, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
40. 大田黒賢也, 紺屋和樹, 寺西亮, 宗藤伸治, 木須隆暢, 金子賢治, 吉積正晃, 和泉輝郎, 磁束ピン止め点を導入したYBa2Cu3Oy超伝導薄膜の生成過程, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
41. 三角和輝, 西山武志, 山田和広, 金子賢治, 池田賢一, 中島英治, 菊池正夫, 高田健, 佐賀誠, 潮田浩作, Al-Mg-Si系合金における析出物および転位の3次元解析, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
42. 橘木雄平, 西山武志, 山田和広, 金子賢治, 伊藤基治, 喜多隆介, フッ素フリーMOD法によるGdBa2Cu3Oy膜の結晶化に及ぼす本焼条件の影響, 日本金属学会・日本鉄鋼協会・軽金属学会九州支部共催平成24年度合同学術講演会, 2012.06.
43. Kenji Kaneko, Takeshi Nishiyama, Kazuhiro Yamada, Takeharu Kato, Teruo Matsushita, Yutaka Yamada, Teruo Izumi, Yuh Shiohara, Nanostructural Characterization of Artificial Pinning Centers in RE-123 Thin Film by Three-dimensional Electron Tomography, MRS Spring, 2012.04.
44. 金子賢治, 福永達也, 中田伸生, 菊池正夫, TEMによるSUS304のその場観察と分析M23C6とCr欠乏層, 日本鉄鋼協会, 2012.03.
45. 福永 達也, 金子 賢治, 中田 伸生, 菊池 正夫, TEM内でのその場加熱による鋭敏化処理と微視的構造解析, 日本鉄鋼協会, 2012.03.
46. K. Kaneko, Electron Tomography to Material Science and Engineering, The 10th Asia-Pacific Microscopy Conference, 2012.02, [URL], 材料工学の分野において、転位、結晶粒、析出物などの微構造解析をはじめ、原子分解能観察や元素分析など、透過型電子顕微鏡(TEM)が日常的に用いられている。しかし、TEMにより得られる情報の多くは薄膜試料から得られた電子の透過像や投影像であり、2次元的な情報しか得ることが出来ない。単純な構造を持つ材料であれば2次元像から3次元的な構造情報を推測することは可能ではあるが、多元系の合金や複合ナノ粒子など、複雑な系では到底困難である。材料の3次元的な微構造が特性を左右することから、材料を3次元で解析することが早くから望まれてきていた。今回、電子線トモグラフィ法を駆使し、金属-複合-セラミックス材料など様々な材料解析をおこなっており、これらの成果を論じた。.
47. 竹田 恵一, 金子 賢治, 北山 幹人, 窒化ケイ素-粒界相界面における希土類イオン偏析現象の解明, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
48. 西山武志 山田和広, 金子賢治, 加藤丈晴, 飛田浩史, 和泉輝郎, 塩原 融, PLD-GdBa2Cu3O7-x中におけるBaHfO3の3次元形態および分散状態の解析, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
49. 和田 勇希, 溝口 航一, 小林 知世, 金子 賢治, 山田 和広, 菊池 正夫, 池田 賢一, 中島 英治, 高田 健, 潮田 浩作, Al-Mg-Si系合金のHVEMによるその場引張試験, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
50. 福永達也, 金子賢治, 山田和広, 中田伸生, 菊池正夫, 鋭敏化したオーステナイト系ステンレス鋼の粒界解析, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
51. Hadi RAZAVI KHOSROSHAHI, 池田 拓之, 齊藤敬高, 中島邦彦, 金子賢治, Y2O3セラミックスの作製および微構造解析, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
52. 佐藤直子, 小島真由美, 諸岡聡, 友田陽, 足立吉隆, 金子賢治, フェライト/マルテンサイトDual-Phase 鋼組織の三次元計量形態評価, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
53. 山田和広, 金子賢治, 吉田悠記, 寺西 亮, 三浦大介, 鈴木浩二, 伊藤基治, 喜多隆介, フッ素フリー有機金属塗布法により作製した GdBa2Cu3Oy薄膜の微構造解析, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
54. 溝口 航一, 金子 賢治, 山田 和広, 和田 勇希, 三角和輝, 菊池 正夫, 池田 賢一, 中島 英治, 高田健, 潮田浩作, 6000系Al合金における析出物の三次元解析, 第53回日本顕微鏡学会九州支部学術講演会, 2011.12, [URL].
55. T. Nishiyama, K. Yamada, K. Kaneko, T. Kato, T. Izumi, Y. Shiohara, Three-Dimensiona Characterization by STEM-Tomography of BZO in YGdBCO, 24th Interntional Symposium on Supserconductivity, 2011.10.
56. R. Kita, K. Kuroda, O. Miura, K. Yamada, K. Kaneko, Effects of TFA addition on the growth of sintered YBa2Cu3Oy superconductrs, 24th Interntional Symposium on Supserconductivity, 2011.10.
57. K. Yamada, K. Kaneko, Y. Yoshida, R. Teranishi, K. Suzuki, M. Itoh, R. Kita, Influence of calcined temperaure on growth of GdBa2Cu3Oy fabricated by F-free MOD, 24th Interntional Symposium on Supserconductivity, 2011.10.
58. H. Tobita, A. Ibi, T. Kato, K. Kaneko, M. Yoshizumi, T. Izumi, Y. Shiohara, IMPROVEMENT OF IN-FIELDS Ic CHARACTERISTICS BY BHO(=BaHfO3) DOPING INTO PLD-GdBCO COATED CONDUCTORS., 24th Interntional Symposium on Supserconductivity, 2011.10.
59. 金子賢治, 電子線トモグラフィによる超伝導特性の解明, 日本顕微鏡学会第55回シンポジウム, 2011.10.
60. K. Kaneko, T. Nishiyama, K. Yamada, T. Kato, T. Matsushita, Y. Yamada, T. Izumi and Y. Shiohara, Three-dimensional nanoscale characterization of various pinning centers in GdBa2Cu3O7-δ-type superconductors, EUCAS Superconductivity Centenial Conference, 2011.09, [URL].
61. 權堂貴志, 香野淳, 田尻恭之, 金子賢治, 山田和広, TiO2ナノ粒子を内包したSBA-15薄膜の物性と膜構造解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
62. 山田和広, 吉田悠記, 金子賢治, 鈴木浩二, 喜多隆介, フッ素フリーMOD法によるGdBa2Cu3Oyの形成過程における微構造解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
63. 西山武志, 山田和広, 金子賢治, 馬場則男, Y1-xGdxBa2Cu3O7-y中におけるBZO3の3次元解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
64. Hadi RAZAVI, 池田拓之, 齋藤敬高, 金子賢治, 中島邦彦, Y2O3セラミックスの作製および微構造解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
65. 和田勇希, 溝口航一, 金子賢治, 山田和広, 菊池正夫, 池田賢一, 中島英治, Al-Mg-Si系合金のHVTEMによるその場引っ張り試験, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
66. 竹田恵一, 金子賢治, 北山幹人, 窒化珪素ー粒界相界面における希土類イオン偏析現象の解明, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
67. 福永達也, 金子賢治, 山田和広, 中田伸生, 菊池正夫, 鋭敏化したオーステナイト系ステンレス鋼の粒界解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
68. 中田京志郎, 髙木健, 助永壮平, 齊藤敬高, 金子賢治, 中島邦彦, 平昭大成, 超微粒子導電性酸化亜鉛粉末の特性評価, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
69. 溝口航一, 和田勇希, 金子賢治, 山田和広, 菊池正夫, 池田賢一, 中島英治, 6000系アルミ合金中の析出物の三次元解析, 日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 共催 平成23年度 合同学術講演大会, 2011.06.
70. 金子賢治, 走査透過電子顕微鏡による粒界偏析の測定, 日本鉄鋼協会 材料の組織と特性部会, 2011.05.
71. K. Kaneko, K. Yamada, S. Sadayama, T. Kato, T. Hirayama, M. Kiuchi, T. Matsushita, Y. Yamada, T. Izumi and Y. Shiohara, Application of Electron Tomography on Superconductors, 5th International Union of Microbeam Analysis Societies, 2011.05, [URL].
72. K. Yamada, T. Nishiyama, K. Kaneko, S. Sadayama, T. Kato, M. Kiuchi, T.Matsushita, M. Yoshizumi, T. Izumi and Y. Shiohara, Three-Dimensional Analysis by Electron Tomography of BaZrO3 Nanoparticles in Y1-xGdxBa2Cu3Oy Superconductor Films, 5th International Union of Microbeam Analysis Societies, 2011.05, [URL].
73. T. Takaki, K. Nakata, N. Saitou, K. Kaneko K. Nakashima and T. Hiraaki, Fabrication and Evaluation of Al-doped ZnO Nano-powders with Low Electrical Resistivity, 5th International Union of Microbeam Analysis Societies, 2011.05, [URL].
74. 西山武志, 山田和広, 金子賢治, 加藤丈晴, 完山正林, 松下照男, 和泉輝朗, 塩原融, Y1-xGdxBa2Cu3O7-y中におけるBZO3の電子線トモグラフィによる解析, 日本顕微鏡学会 第67回学術講演会, 2011.05.
75. 山田和広, 金子賢治, 吉田悠記, 鈴木浩二, 喜多隆介, フッ素フリー塗布熱分解法によるGdBa2Cu3Oy膜の微構造に及ぼす仮焼温度の影響, 日本顕微鏡学会 第67回学術講演会, 2011.05.
76. 福永達也, 金子賢治, 山田和広, 中田伸生, 菊池正夫, 鋭敏化したオーステナイト系ステンレス鋼の粒界解析, 日本顕微鏡学会 第67回学術講演会, 2011.05.
77. 和田勇希, 金子賢治, 山田和広, 溝口航一, 菊池正夫, 池田賢一, 中島英治, Al-Mg-Si系合金のHVTEMによるその場引っ張り試験, 日本顕微鏡学会 第67回学術講演会, 2011.05.
78. 竹田恵一, 金子賢治, 北山幹人, 窒化珪素ー粒界相界面における希土類イオン偏析現象の解明, 日本顕微鏡学会 第67回学術講演会, 2011.05.
79. 溝口航一,金子賢治, 山田和広, 和田勇希, 菊池正夫, 池田賢一, 中島英治, 6000系アルミ合金中の析出物の3次元解析, 日本顕微鏡学会 第67回学術講演会, 2011.05.
80. 山田和広, 安田恭野, 内田聡, 古君修, 金子賢治, 2相組織鋼におけるナノインデンテーション法により導入された塑性域の解析, 日本顕微鏡学会 第67回学術講演会, 2011.05.
81. 柳本翼, 金子賢治, Yeon-tae Yu, Au-SnO2コアシェル型ナノ粒子のTEMによる構造解析, 顕微鏡学会九州支部会, 2010.12.
82. 山田和広, 金子賢治, 吉田悠記, 完山正林, 大久保理香, 竹内稔晃, 喜多隆介, BaTbO3添加YBa2Cu3Oy焼結体のFIB-SEMおよびTEMによる解析, 顕微鏡学会九州支部会, 2010.12.
83. 西山武志, 山田和広, 金子賢治, 加藤丈晴, 完山正林, 木内勝, 松下照男, 吉積正晃, 和泉輝朗, 塩原融, MOD法により作成されたYGdBCOにおけるBZOの電子線トモグラフィによる解析, 顕微鏡学会九州支部会, 2010.12.
84. 金子賢治, 結晶材料の解析, マテリアル電子線トモグラフィ研究部会, 2010.11.
85. K. Kaneko, K. Furuya, K. Yamada, S. Sadayama, J. S. Barnard, P. A. Midgley, T. Kato and T. Hirayama, M. Kiuchi, T. Matsushita, Y. Yamada, T. Izumi, Y. Shiohara, 3-D Microstructural analysis of Coated Conductors with APC, 23rd International Symposium on Superconductivity, 2010.11, [URL], 走査透過型電子顕微鏡と電子線トモグラフィ法を組み合わせることにより、従来不可能とされていた超伝導材料中の人工ピンニングセンターを立体的に可視化することに成功した。3次元情報を得るのみならず、角度情報、サイズ、体積率といった様々3次元情報を取得することに成功し、超伝導特性と微構造の相関を解明することに成功している。.
86. R. Teranishi, K. Shiohara, Y. Masuda, K. Yamada, N. Mori, M. Mukaida, S. Munetoh, K. Kaneko, M. Inoue, T. Kiss, M. Yoshizumi, T. Izumi, S. Awaji, Flux Pinning Properties of YBCO films with Sn compounds by a MOD method using TFA salts, 23rd International Symposium on Superconductivity, 2010.11, [URL].
87. K. Yamada, T. Nishiyama, K. Kaneko, S. Sadayama, T. Kato, M. Kiuchi, T. Matsushita, M. Yoshizumi, T. Izumi, Y. Shiohara, 3D Visualization by STEM-Tomography of BZO in YGdBCO, 23rd International Symposium on Superconductivity, 2010.11, [URL].
88. T.Iwasa, R. Kita, O. Miura, A. Ichinose, K. Yamada, K. Kaneko, S. Horii, Fabrication of (Eu,RE)Ba2Cu3Oy (RE=Gd and Sm) Films by MOD using Metal 2-Ethylhexanates, 23rd International Symposium on Superconductivity, 2010.11, [URL].
89. R. Kita, K. Suzuki, T. Takeuchi, T. Iwasa, O. Miura, K. Yamada, K. Kaneko, A. Ichinose, Stable Barium Ccompounds in YBa2Cu3Oy Superconductors for Artificial Pinning Centers, 23rd International Symposium on Superconductivity, 2010.11, [URL].
90. T. Maebatake, Y. Ichinose, K. Yamada, N. Mori, R. Teranishi, M. Mukaida, S. Munetoh, T. Kiss, M. Inoue, K. Kaneko, M. Yoshizumi, T. Izumi, Joint Properties of REBCO Coated Conductors, 23rd International Symposium on Superconductivity, 2010.11, [URL].
91. K. Kaneko, K. Yamada, S. Sadayama, J. S. Barnard, P. A. Midgley, T. Kato, T. Hirayama, M. Kiuchi, T. Matsushita, Y. Yamada, T. Izumi and Y. Shiohara, TEM analysis of the nanostructure in coated conductors, International Workshop on Coated Conductors for Applications (CCA 2010), 2010.10, [URL].
92. Y. Masuda, Y. Miyanaga, R. Teranishi, K. Yamada, N. Mori, M. Mukaida, T. Kiss, M. Inoue, M. Yoshizumi, T. Izumi, K. Kaneko, S. Munetoh, Flux pinning properties of YBCO films with Sn compound addition by TFA-MOD method, Japan-Korea Superconductivity Workshop, 2010.10, [URL].
93. 山田和広, 西山武志, 金子賢治, 加藤丈晴, 完山正林, 木内勝, 松下照男, 吉積正晃, 和泉輝郎, 塩原融, MOD-YGdBCOにおけるBZOの電子線トモグラフィ法による3次元可視化, 日本金属学会 秋期(第147回)大会, 2010.09.
94. K. Kaneko, K. Yamada, S. Sadayama, J. S. Barnard, P. A. Midgley, T. Kato, T. Hirayama, M. Kiuchi, T. Matsushita, Y. Yamada, T. Izumi and Y. Shiohara, 3D analysis of pinning centers in superconductive GdBa2Cu3O7-x, 17th International Microscopy Congress, 2010.09, [URL].
95. S. Sadayama, N. Suzuki, K. Yamada, K. Kaneko, 3D analysis on Al-Mg-Mn-Sc-Zr alloy using DualBeam tomography, 17th International Microscopy Congress, 2010.09, [URL].
96. T. Takaki, K. Kurosawa, S. Sukenaga, N. Saito, H. Razavi, K. Kaneko, K. Nakashima, E. Okunishi and T. Hiraaki, Electrolytic synthesis of Al-doped ZnO powders with low electrical resistivity, 17th International Microscopy Congress, 2010.09.
97. H. Razavi, K. Yamada, T. Katayama, N. Saito, K. Nakashima and K. Kaneko, Fabrication and Characterization of Mo-SiO2 Composite, 17th International Microscopy Congress, 2010.09.
98. S. Hata, M. Mitsuhara, M. Tanaka, K. Kaneko, K. Higashida, K. Ikeda, H. Nakashima and S. Matsumura, Development of 3D TEM Imaging Techniques Using Diffraction Contrast, 17th International Microscopy Congress, 2010.09.
99. 松下和輝, 喜多隆介, 岩佐俊彦, 三浦大介, 一瀬中, 山田和広, 金子賢治, 堀井滋, フッ素フリーMOD-GdBCO 超伝導薄膜の厚膜化検討, 2010年秋季 第71回 応用物理学会学術講演会, 2010.09, [URL].
100. 咲本健太, 喜多隆介, 岩佐俊彦, 三浦大介, 一瀬中, 山田和広, 金子賢治, 堀井滋, フッ素フリーMOD-GdBCO 超伝導薄膜へのIn 添加効果, 2010年秋季 第71回 応用物理学会学術講演会, 2010.09, [URL].
101. 岩佐俊彦, 喜多隆介, 三浦大介, 一瀬中, 山田和広, 金子賢治, 堀井滋, 金属オクチル酸塩を用いたMOD 法によるEu 系超伝導薄膜へのGd, Sm 混晶化効果, 2010年秋季 第71回 応用物理学会学術講演会, 2010.09, [URL].
102. K. Ikeda, K. Terada, S. Hata, H. Nakashima, K. Takata, M. Saga, J. Takahashi, K. Ushioda, K. Kaneko and M. Kikuchi , Effect of cluster and precipitate on tensile property in Al-Mg-Si alloy, ICAA12, 2010.09, [URL].
103. K. Takata, M. Saga, J. Takahashi, K. Ushioda, K. Ikeda, K. Terada, S. Hata, H. Nakashima, K. Kaneko and M. Kikuchi, Analysis of yield strength for isothermal aged Al-Mg-Si alloys, ICAA12, 2010.09, [URL].
104. K. Kaneko, Application of electron tomography for characterizing precipitate morphologies in Al alloys, ICAA12, 2010.09, [URL], 走査透過型電子顕微鏡と電子線トモグラフィ法を組み合わせることにより、従来不可能とされていたアルミニウム合金中の析出物を立体的に可視化することに成功した。3次元情報を得るのみならず、サイズ、体積率といった様々3次元情報を取得することに成功し、機械的特性と微構造の相関を解明することに成功している。.
105. 金子賢治, 電顕トモグラフィ理論, 第21回 電顕サマースクール, 2010.07.
106. T. Takaki, K. Kurosawa, S. Sukenaga, N. Saito, H. Razavi, K. Kaneko, K. Nakashima, E. Okunishi and T. Hiraaki, Electrolytic synthesis of Al-doped ZnO powders with low electrical resistivity, The 2nd International Conference of Advanced Microscopy and Theoretical Calculations, 2010.06.
107. H. Razavi, K. Yamada, T. Katayama, N. Saito, K. Nakashma, K. Kaneko, Fabrication and Characterization of Mo-SiO2 Composite, The 2nd International Conference of Advanced Microscopy and Theoretical Calculations, 2010.06, [URL].
108. K. Kaneko, K. Yamada, S. Sadayama, J. S. Barnard, P. A. Midgley, T. Kato, T. Hirayama, M. Kiuchi, T. Matsushita, Y. Yamada, T. Izumi and Y. Shiohara, 3D analysis of pinning centers in superconductive GdBa2Cu3O7-x, The 2nd International Conference of Advanced Microscopy and Theoretical Calculations, 2010.06, [URL].
109. Hadi Razavi Khosroshahi, 山田和広, 片山智之, 齊藤敬高, 中島邦彦, 金子賢治, Mo-SiO2複合材料の作製及び微構造解析, 合同学術講演会, 2010.06.
110. 柳本翼, Razavi Hadi, 金子賢治, 林靖彦, Bongyong Jang, 野村侑生, 徳永智春, 奥西栄治, Co/Pd内包カーボンナノチューブのTEMによる構造解析, 合同学術講演会, 2010.06.
111. 山田和広, 古屋和基, 金子賢治, 完山正林, 加藤丈晴, 松下照男, 山田 穣, 和泉輝郎, 塩原 融, GdBCO超電導体における人工ピニングセンタの3次元電子線トモグラフィ法による定量解析, 合同学術講演会, 2010.06.
112. 竹田恵一, 金子賢治, 山田和広, 目 義雄, 奥山秀男, RFプラズマ法で作製したTiO2ナノ複合材料のTEMによる構造解析, 合同学術講演会, 2010.06.
113. 西山武志, 金子賢治, 有田稔彦, 阿尻雅文, ポリスチレンにより表面を修飾したTiO2,TiNナノ粒子のTEMによる解析, 合同学術講演会, 2010.06.
114. 山田和広, 金子賢治, 完山正林, 池田賢一, 中島英治, Al-4.5Mg-0.7Mn-0.3Sc-0.2Zr合金におけるAl3(Sc,Zr)の微構造解析, 日本顕微鏡学会 第66回学術講演会, 2010.05.
115. 完山正林, 鈴木直久, 山田和広, 金子賢治, DualBeamによるAl-Mg-Mn-Sc-Zr合金中析出物の三次元再構築, 日本顕微鏡学会 第66回学術講演会, 2010.05.
116. 柳本翼, Razavi Hadi, 金子 賢治, 林靖彦, Bongyong Jang, 徳永智春, 奥西 栄治, Co/Pd内包カーボンナノファイバーの微構造解析, 日本顕微鏡学会 第66回学術講演会, 2010.05.
117. 高木健, 黒澤慶子, Hadi Razavi, 助永壮平, 齊藤敬高, 金子賢治, 中島邦彦, 電解合成法による超微粒子導電性酸化亜鉛の作製, 日本金属学会 春期(第146回)大会, 2010.03.
118. 山田和広, 古屋和基, 金子賢治, 加藤丈晴, 完山正林, 松下照男, 山田穣, 和泉輝郎, 塩原融, GdBCO超電導線材におけるBZO磁束ピン止めセンターの電子線トモグラフィ法による3次元解析, 日本金属学会 春期(第146回)大会, 2010.03.
119. 山田和広, 古屋和基, 金子賢治, 完山正林, 加藤丈晴, 松下照男, 山田穣, 和泉輝郎, 塩原融, GdBCO超電導膜におけるBZOナノロッドのSTEM-CT法による3次元解析, 第57回応用物理学関係連合講演会, 2010.03.
120. 金子賢治, 電子線トモグラフィ法による結晶性材料の解析, 2009年度NIMSナノ計測センターシンポジウム, 2010.02.
121. S. Sadamatsu, Masaki Tanaka, K. Higashida, Kenji Kaneko, Masatoshi Mitsuhara, Satoshi Hata, M. Honda, Crack tip dislocations observed by combining scanning transmission electron microscopy and computed tomography, 6th International Conference on Processing and Manufacturing of Advanced Materials - THERMEC'2009, Crack tip dislocations and dislocations introduced by three point-bending tests at high temperature are observed by combinating scanning transmission electron microscopy and computed tomography (STEM-CT). Commercially available P type (001) single crystal silicon wafers were employed. A series of STEM image was acquired from -60° to +60° in tilt range with 2° in tilt step. The diffraction vector was maintained close to g(hkl) = 220 during the acquisition by adjusting the [110] direction of the sample parallel to the tilt axis of the holder. Reconstructed images of dislocations revealed dislocation structures in three-dimension..
122. 柳本翼, Hadi Razavi, 金子賢治, 林靖彦, Bongyong Jang, 徳永智春, Co/Pd 内包カーボンナノファイバーの微構造解析, 第51回 日本顕微鏡学会 九州支部総会・学術講演会, 2009.12.
123. Hadi Razavi, 金子賢治, 阿部浩也, 野間淳一, アークプラズマ法により作製したFe-Cナノ粒子のTEMによる構造解析, 第51回 日本顕微鏡学会 九州支部総会・学術講演会, 2009.12.
124. 古屋和基, 金子賢治, 山田和宏, 加藤丈晴, 完山正林, 松下照男, 超電導中の人工ピン止め点の3次元解析, 第51回 日本顕微鏡学会 九州支部総会・学術講演会, 2009.12.
125. 金子賢治, 電子線トモグラフィ法による金属材料の3D解析, 製銑第54委員会 第175回研究会, 2009.12.
126. 金子賢治, 電子線トモグラフィ法による結晶性材料の解析とその応用例 ・・異方性と特性・・, 【日本顕微鏡学会】第3回 電子線トモグラフィ法チュートリアル, 2009.11.
127. 山田和広、金子賢治、周致霆、門池田賢一、中島英治, Al-4.5Mg-0.7Mn-0.3Sc-0.2Zr 合金における析出物の3D-ET 法による可視化, 軽金属学会, 2009.11, [URL].
128. 池田賢一, 高下拓也, 波多聰, 中島英治, 山田和広, 金子賢治, Al-0.5Mg-0.5Si-0.3Sc-0.2Zr合金の再結晶粒成長挙動, 軽金属学会, 2009.11, [URL].
129. K. Kaneko, Characterization of various crystalline materials by 3D-ET, 第11回全北大学—九州大学合同国際シンポジウム, 2009.11.
130. K. Yamada, K. Furuya, R. Hadi, K. Kaneko, S. Sadayama, T. Kato, T. Matsushita, A. Ibi, Y. Yamada, T. Izumi, Y. Shiohara, Three-Dimensional Characterization of BZO Nanorods in a GdBCO Coated Conductor by TEM-CT, 22nd International Symposium on Superconductivity, 2009.11, [URL].
131. 池田賢一、高下拓也、波多聰、中島英治、山田和広、金子賢治, Al-Mg-Si系合金の集合組織形成に及ぼすScとZr添加の影響, 軽金属学会「集合組織研究部会」, 2009.10, [URL].
132. K. Kaneko, Application of electron tomography on alloys, The 4th KIMS-Kyushu University Joint Symposium on Steel Research, 2009.10.
133. K. Kaneko, Multi-dimensional characterizations of materials by TEM, FEMMS, 2009.10.
134. K. Yamada, K. Furuya, R. Hadi, K. Kaneko, J. S. Barnard, P. A. Midgley, S. Sadayama, T. Kato, Y. Yamada, T. Izumi, Y. Shiohara, Three-Dimensional Characterization by TEM-CT of Pinning Centers in a GdBa2Cu3O7-y Superconductor Film, FEMMS, 2009.09.
135. 山田和広, 古屋和基, 金子賢治, 完山正林, 加藤丈晴, 松下照男, 衣斐顕, 山田穣, 和泉輝郎, 塩原融, BZO ナノロッド分散GdBCO 線材のTEM-CT 法による3 次元可視化, 日本金属学会秋期(第145回)大会, 2009.09.
136. 池田 賢一, 高下 拓也, 波多 聰, 中島 英治, 山田 和広, 金子 賢治, Sc, Zr複合添加Al-Mg-Si系合金板の再結晶組織, 日本金属学会秋期(第145回)大会, 2009.09.
137. HADI RAZAVI, 金子賢治, 阿部浩也, アークプラズマ法により作製したFe-Cナノ粒子のTEMによる構造解析, 日本金属学会秋期(第145回)大会, 2009.09.
138. 柳本翼, 金子賢治, 林靖彦, Bongyong Jang, 徳永智春, Co/Pd 内包カーボンナノチューブのTEM による構造解析, 日本金属学会秋期(第145回)大会, 2009.09.
139. 金子 賢治, 材料系3D-TEMの現状とこれから, 日本鉄鋼協会秋季(第158回) 大会, 2009.09.
140. 中村達徳, 喜多隆介, 三浦大介, 一瀬中, 山田和広, 金子賢治, MOD-Sm0.33Eu0.33Gd0.33Ba2Cu3Oy膜作製における焼成雰囲気依存性, 秋季(第70回)応用物理学会, 2009.09.
141. 山田和広, 金子賢治, 中村達徳, 喜多隆介, GdBCO膜における第2相化合物の電子線トモグラフィ法による3次元可視化, 秋季(第70回)応用物理学会, 2009.09.
142. 細谷有功, 中村達徳, 喜多隆介, 三浦大輔, 一瀬中, 山田和広, 金子賢治, 堀井滋, MOD-GdBCO膜中における人工ピン形成に関する検討, 秋季(第70回)応用物理学会, 2009.09.
143. 大野真史, 中村達徳, 喜多隆介, 三浦大輔, 一瀬中, 山田和広, 金子賢治, 金属オクチル酸塩を用いたMOD法による(Sm,Ho)BCO膜の作製, 秋季(第70回)応用物理学会, 2009.09.
144. 鈴木進也, 中村達徳, 喜多隆介, 三浦大介, 一瀬中, 山田和広, 金子賢治, F-free溶液を用いたMOD-(Nd,Eu,Gd)Ba2Cu3Oy膜へのEr混晶化効果, 秋季(第70回)応用物理学会, 2009.09.
145. 柳本翼, HADI RAZAVI, 金子賢治, 林靖彦, Bongyong Jang, 徳永智春, Co/Pd 内包カーボンナノチューブのTEM による構造解析, 分析電子顕微鏡討論会, 2009.09.
146. HADI RAZAVI, 金子賢治, 阿部浩也, アークプラズマ法により作製したFe-Cナノ粒子のTEMによる構造解析, 平成21年度合同学術講演会, 2009.06.
147. 柳本翼, 金子賢治, 林康彦, Bongyong Jang, 徳永智春, Co/Pd内包カーボンナノチューブのTEMによる構造解析, 平成21年度合同学術講演会, 2009.06.
148. 古屋和基, 山田和広, 金子賢治, 加藤丈晴, 完山正林, 松下照男, GdBCO-BZO超伝導線材中ピン止めセンターの三次元可視化, 平成21年度合同学術講演会, 2009.06.
149. 秦哲郎, 金子賢治, 有田俊彦, 阿尻雅文, 超高圧EF-TEMによる高空間分解能EF像取得の試み, 平成21年度合同学術講演会, 2009.06.
150. 山田和広, 金子賢治, 池田賢一, 中島英治, Sc,Zr添加Al-Mg-Si合金時効材のTEMによる微細組織観察, 平成21年度合同学術講演会, 2009.06.
151. 秦哲郎, 金子賢治, 有田稔彦, 阿尻雅文, 超高圧EF-TEM による高空間分解能EF 像取得の試み, 日本顕微鏡学会, 2009.05.
152. 金子賢治, 北脇高太郎, 奥山秀男, 宇田雅広, 目義雄, アークプラズマ法により生成したTiN 系複合ナノ粒子の構造解析, 日本顕微鏡学会, 2009.05.
153. 古屋和基, 山田和広, 金子賢治, 加藤丈晴, 完山正林, 松下照男, GdBCO-BZO 超電導線材中のピン止めセンターの三次元可視化, 日本顕微鏡学会, 2009.05.
154. 完山正林, 関口浩美, 青山一弘, 金子賢治, 半導体試料の電子線トモグラフィ法による解析, 日本顕微鏡学会, 2009.05.
155. 奥山秀男, 宇田雅広, 目義雄, 北脇高太郎, 金子賢治, TiN-Ag複合ナノ粒子の製造法とその形態, 粉体工学会 春期研究発表会, 2009.05.
156. 池田賢一, 高下拓也, 波多 聰, 中島英治, 山田和広, 金子賢治, Al-Mg-Si系合金の再結晶挙動に及ぼすScとZr添加の影響, 軽金属学会 第116回春期大会, 2009.05.
157. 池田賢一, 高下拓也, 光原昌寿, 波多聡, 中島英治, 山田和広, 金子賢治, Sc,Zr複合添加Al-Mg-Si系合金熱間圧延板の析出形態, 日本金属学会, 2009.03.
158. 金子賢治, 電子線トモグラフィによる様々な結晶性材料の解析, 日本顕微鏡学会 関東支部会, 2009.03.
159. 杉川幸太, 土屋陽一, 白木智丈, 金子賢治, 佐田和己, 新海征治, 半人工多糖をテンプレート分子としたナノ構造体の構築, 日本化学会第89春季年会, 2009.03.
160. Kenji Kaneko, Characterization of various crystalline materials by three-dimensional electron tomography, Asia-Pacific Congress on Electron Tomography, 2009.02, [URL].
161. 金子賢治, 電子線トモグラフィによる様々な材料の解析, 日本顕微鏡学会・生体構造解析分科会, 2009.01.
162. 田中將己, 東田賢二, 金子賢治, STEM-LAADFを用いた材料解析, 日本顕微鏡学会・デバイス分科会, 2008.12.
163. 金子賢治, 3次元電子線トモグラフィ法の応用例, 日本顕微鏡学会・デバイス分科会, 2008.12.
164. 秦哲郎, 金子賢治, 徳永智春, 堀田善治, HPT法による添加量の異なるAl-Mg合金の作製とその解析, 第50回日本顕微鏡学会九州支部総会・学術講演会, 2008.12.
165. 北脇高太郎, 金子賢治, 山田和広, 奥山秀男, 宇田雅広, 目義雄, アークプラズマ法により生成された複合ナノ粒子の構造解析, 第50回日本顕微鏡学会九州支部総会・学術講演会, 2008.12.
166. 本田雅幹, 定松直, 田中將己, 金子賢治, 東田賢二, 光原昌寿, 波多聡, 亀裂先端転位群の電子線トモグラフィ観察, 第50回日本顕微鏡学会九州支部総会・学術講演会, 2008.12.
167. 山田和広, 高下拓也, 池田賢一, 中島英治, 金子賢治, Al-Mg-Si-Sc-Zr合金のベークハードに及ぼす前処理条件の検討, 第50回日本顕微鏡学会九州支部総会・学術講演会, 2008.12.
168. M. Tanaka, M. Honda, M. Mitsuhara, S. Hata, K. Kaneko, and K. Higashida, Three-dimensional analyses of crack tip dislocations observed by electron tomography, 9th Asia-Pacific Microscopy Conference, 2008.11, [URL].
169. K. Kaneko, Three-dimensional nano characterization of catalytic materials by TEM, 9th Asia-Pacific Microscopy Conference, 2008.11, [URL].
170. K. Kitawaki, K. Kaneko, K. Inoke, J. C. Hernandez, P. A. Midgley, H. Okuyama, M. Uda and Y. Sakka, Fabrication and Characterization of TiN-Ag Nano-Dice, 9th Asia-Pacific Microscopy Conference, 2008.11, [URL].
171. K. Kurihara, T. Hashishin, J. Tamaki, K. Kaneko, Hydrothermal Synthesis of Pd Loaded SnO2 Nano-particles and Their Methane Sensing Properties, PRiME2008, 2008.10, [URL].
172. 伊藤正寛, 名嘉節, 張静, 金子賢治, 川添良幸, 阿尻雅文, 有機分子修飾セリアナノ粒子の物性変化に関する第一原理計算, 第40回化学工学会秋季大会, 2008.09.
173. 杉川幸太, 沼田宗典, 土屋陽一, 金子賢治, 佐田和己, 新海征治, 機能性多糖を用いたカーボンナノチューブの組織体形成と形状制御, 第57回高分子討論会, 2008.09.
174. 刀祢裕介, 藤田典史, 金子賢治, 佐田和己, 新海征治, オルガノゲルを鋳型とした金ナノ構造体の構築, 第57回高分子討論会, 2008.09.
175. 栗原圭一, 橋新 剛, 玉置 純, 金子賢治, 水熱法によるパラジウム担持酸化物ナノ粒子の合成とその微細構造観察, 第102回触媒討論会, 2008.09, [URL].
176. 古屋和基, 金子 賢治, 野村要平, 石原達己, 小野寺恒信, 及川英俊, 笠井均, 馬場則男, フタロシアニンと白金を用いたナノハイブリッド材料の微構造解析, 日本金属学会, 2008.09.
177. 秦哲郎, 金子賢治, 堀田善治, HPT法による添加量の異なるAl-Mg合金の作製とその解析, 日本金属学会, 2008.09.
178. 金子賢治, 3次元電子線トモグラフィ法によるAl合金中の析出物の評価, 湯川記念講演会・討論会, 2008.09.
179. 金子賢治, 北脇高太郎, 張静, 大原智, 阿尻雅文, アンナ・ハンガリア, ポール・ミッジレー, 3次元電子線トモグラフィ法による触媒ナノ粒子の微細構造評価, 日本セラミックス協会, 2008.09.
180. 金子賢治, 透過型電子顕微鏡で3次元を観る, 日本分析化学会, 2008.09.
181. 杉川幸太, 沼田宗典, 金子賢治, 佐田和己, 新海征治, 機能化多糖を用いたカーボンナノチューブの組織化, 第25回有機合成化学セミナー, 2008.09.
182. 秦哲朗, 金子賢治, 徳永智春, 堀田善治, HPT法によるAl-Mg過飽和固溶体の作製とその解析, 日本顕微鏡学会 分析電子顕微鏡討論会, 2008.09.
183. 金子賢治, 3Dトモグラフィの基礎と応用, 日本顕微鏡学会 分析電子顕微鏡討論会, 2008.09.
184. K. Kaneko, Characterization of Precipitates in Al Alloys by three-dimensional electron tomography, NCEM seminar, 2008.08.
185. K. Kaneko, K. Furuya, K. Kitawaki, T. Onodera, H. Kasai, H. Oikawa, Y. Nomura, T. Ishihara, A.B. Hungria, J.-C. Hernandez-Garrido, P.A. Midgley, Nanostructural characterization of Pt nanoparticles on phthalocyanine, The 1st International Symposium on Advanced Microscopy and Theoretical Calculations, 2008.06, [URL].
186. 杉川 幸太, 土屋 陽一, 沼田 宗典, 金子 賢治, 佐田 和己, 新海 征治, イオン性基修飾カードランを用いたカーボンナノチューブカプセルの創製, 第3回ホスト・ゲスト化学シンポジウム, 2008.05.
187. 古屋和基, 金子賢治, 野村要平, 石原達己, 小野寺恒信, 及川英俊, 笠井均, 馬場則男, フタロシアニンと白金を用いたハイブリッドナノ結晶の微細構造解析, 日本顕微鏡学会, 2008.05.
188. 金子賢治, 佐藤圭介, 徳永智春, 林靖彦, Al-(Ge,Si)析出合金を利用した半導体ナノワイヤの作製とその解析, 日本顕微鏡学会, 2008.05.
189. 北脇高太郎, 金子賢治, 奥山秀男, 宇田雅広, 目義雄, アークプラズマ法により生成された複合ナノ粒子の構造解析, 日本顕微鏡学会, 2008.05.
190. 田中將己、本田雅幹、光原昌寿、波多聡、金子賢治、東田賢二, 亀裂先端転位の三次元構造観察, 日本顕微鏡学会, 2008.05.
191. 金子賢治, 3次元電子線トモグラフィの金属への応用, 日本顕微鏡学会 電子線トモグラフィ研究部会, 2008.05.
192. 忰山高大, 若林里衣, 竹林新二, 金子賢治, 竹内正之, 新海征治, 超分子化学的手法を用いた共役系高分子の配列制御(1), 日本化学会第88春季年会, 2008.03.
193. 忰山高大, 竹林新二, 若林里衣, 金子賢治, 竹内正之, 新海征治, 超分子化学的手法を用いた共役系高分子の配列制御(2), 日本化学会第88春季年会, 2008.03.
194. 為末真吾, 沼田宗典, 金子賢治, 新海征治, 多糖・シゾフィランによるラッピングとボロン酸架橋をキープロセスとした高分子集合体の形成, 日本化学会第88春季年会, 2008.03.
195. 杉川幸太, 沼田宗典, 金子賢治, 新海征治, 静電相互作用部位を有するらせん状多糖をホストとした機能性分子の会合形態制御, 日本化学会第88春季年会, 2008.03.
196. 南豪, 金子賢治, 長崎健, 久保由治, 疎水性アニオンに対して比色応答性を示す両親媒性イソチオウロニウム被覆型金ナノ粒子の合成とフッ化物イオン検出への展開, 日本化学会第88春季年会, 2008.03.
197. 刀祢裕介, 藤田典史, 金子賢治, 新海征治, 低分子ゲルの一次元空孔を利用した金属微粒子の合成, 日本化学会第88春季年会, 2008.03.
198. 古屋和基, 金子賢治, 野村要平, 石原達己, 矢口雄介, 小野寺恒信, 及川英俊, 笠井均, ハイブリッド系有機―金属ナノ結晶の微細構造解析, 日本金属学会, 2008.03.
199. 田中將己, 金子賢治, 東田賢二, 光原昌寿, 波多聡, 電子線トモグラフィによる亀裂先端転位の三次元構造解析, 日本金属学会, 2008.03.
200. 北脇高太郎, 金子賢治, 堀田善治, Zhang Jing, 大原智, 阿尻雅文, 3次元電子線トモグラフィによるCeO2ナノ粒子の微構造解析, 日本金属学会, 2008.03.
201. 松村晶, 安田和弘, 大尾岳史, 田中英志, 友清芳二, 桑野範之, 板倉賢, 波多聰, 大上悟, 金子賢治, 大崎光明, 応本和也, 大田繁正, 松下光英, 畦田俊司, 超高圧電子顕微鏡JEM-1300NEFの新しい機能, 第49回日本顕微鏡学会九州支部総会・学術講演会, 2007.12.
202. 森川龍也, 東田賢二, 金子賢治, 川村能人, 竹中雅紀, 木下大輔, 長周期構造相を含むマグネシウム合金の組織と力学特性, 第49回日本顕微鏡学会九州支部総会・学術講演会, 2007.12.
203. 佐藤圭介, 金子賢治, 堀田善治, 徳永智春, 林靖彦, Al-Ge,Al-Si合金を利用した半導体ナノワイヤの作製, 第49回日本顕微鏡学会九州支部総会・学術講演会, 2007.12.
204. 北脇高太郎, 金子賢治, 堀田善治, Zhang Jing, 大原智, 阿尻雅文, 水熱合成法で得られたCeO2ナノ粒子の微構造解析, 第49回日本顕微鏡学会九州支部総会・学術講演会, 2007.12.
205. 田中將己, 金子賢治, 東田賢二, 光原昌寿, 波多聰, ADF法を用いた転位の3次元構造観察, 第49回日本顕微鏡学会九州支部総会・学術講演会, 2007.12.
206. Kenji Kaneko, Keisuke Sato, Zenji Horita, Koji Inoke, Characterization of precipitates by three-dimensional electron tomography, 6th Pacific Rim International Conference on Advanced Materials and Processing, PRICM 6, 2007.11, [URL], Structures and morphologies of Ge precipitates in an Al-Ge alloy were characterized by a combination of transmission electron microscopy and three-dimensional electron tomography. Faceting of the precipitates was clearly seen using transmission electron microscopy and varieties of precipitate morphologies were identified by three-dimensional electron tomography..
207. Kenji KANEKO, Three-dimensional nano characterization of materials by TEM, 韓国電子顕微鏡学会, 2007.11.
208. 金子賢治, TEMによる3次元解析, TEM最新技術セミナー, 2007.11.
209. 金子賢治, 3次元電子線トモグラフィによる金属材料の評価, 日本顕微鏡学会, 2007.10.
210. 金子賢治, ナノ粒子の三次元構造評価の新展開, 粉体接合プロセス研究会, 2007.10.
211. 金子賢治, Transmission Electron Microscopy with computed tomography A best tool for characterizing nanoscale materials in 3D, The 1st International Symposium for Future Molecular Systems, 2007.10, [URL].
212. 小西 克明, 平谷卓之, 久保美菜子, 八巻明裕, 岩本多加志, 金子賢治, 表面での分子認識に誘起される半導体CdSクラスターの発光応答, 第60回コロイドおよび界面化学討論会, 2007.09.
213. 柴田誠之, 田中智史, 池田朋宏, 竹林 新二, 平田修, 金子賢治, 竹内正之, 新海 征治, 回転部位を有するポルフィリンポリマーの分子認識挙動, 第56回高分子討論会, 2007.09.
214. 杉川幸太, 沼田宗典, 池田将, 金子賢治, 新海征治, イオン性基修飾カードランを用いた機能性分子の配列制御, 第56回高分子討論会, 2007.09.
215. 為末真吾, 沼田宗典, 金子賢治, 櫻井和朗, 新海征治, 多糖・シゾフィランによるラッピングとホウ酸架橋をキープロセスとしたSWNT の階層化, 第56回高分子討論会, 2007.09.
216. 北脇高太郎, 金子賢治, 堀田善治, Zhang Jing, 大原智, 阿尻雅文, 水熱合成法で得られたCeO2ナノ粒子の微構造解析, 日本金属学会秋期講演大会, 2007.09.
217. 佐藤圭介, 金子賢治, 徳永智春, 堀田善治, 林靖彦, Ge,Si添加Al合金を利用した半導体ナノワイヤの作製, 日本金属学会秋期講演大会, 2007.09.
218. 金子賢治, 3次元電子線トモグラフィによる材料解析, 日本顕微鏡学会/分析電子顕微鏡分科会, 2007.08, [URL].
219. 金子賢治, 電子線トモグラフィ法による結晶性材料の解析, 日本顕微鏡学会, 2007.05.
220. 竹林 新二, 久保 羊平, 金子 賢治, 竹内 正之, 新海 征治, 超分子化学的手法を用いた共役系高分子の配列制御(1), 日本化学会第87春季年会, 2007.03.
221. 忰山 高大, 久保 羊平, 金子 賢治, 竹内 正之, 新海 征治, 超分子化学的手法を用いた共役系高分子の配列制御(2), 日本化学会第87春季年会, 2007.03.
222. 柴田誠之, 田中智史, 池田朋宏, 竹林新二, 平田修, 竹内正, 新海征治, 金子賢治, 回転運動の制御による情報伝達システムの構築(2), 日本化学会第87春季年会, 2007.03.
223. 沼田宗典, 藤沢友久, 櫻井和朗, 新海征治, 金子賢治, 小西利史, 和田達夫, 機能性マテリアルを指向したβ1,3-glucan/SWNTナノコンポジットの創製とその階層化, 日本化学会第87春季年会, 2007.03.
224. 為末真吾, 沼田宗典, 金子賢治, 櫻井和朗, 新海征治, 多糖・シゾフィランによるラッピングとホウ酸架橋をキープロセスとしたSWNTの階層化, 日本化学会第87春季年会, 2007.03.
225. 杉川幸太, 沼田宗典, 池田将, 櫻井和朗, 新海征治, 金子賢治, イオン性基修飾カードラン-SWNT複合体の形成とその階層構造制御, 日本化学会第87春季年会, 2007.03.
226. MALIK Sudip, 藤田典史, 後藤佑太, 金子賢治, 新海征治, 有機固溶体を用いたフラーレンの一次元配列とその重合, 日本化学会第87春季年会, 2007.03.
227. 原口修一, 沼田宗典, 池田将, 金子賢治, 櫻井和朗, 新海征治, ホスト機能を持つ多糖をインターフェースとした有機無機ナノコンポジットの創製, 日本化学会第87春季年会, 2007.03.
228. 内藤綱彦, 渡邉啓, 林靖彦, 徳永智春, 金子賢治, メタン・水素ガスをもちいたマイクロ波プラズマ化学気相成長法による垂直配向したカーボンナノチューブの成長, 第32回フラーレン・ナノチューブ総合シンポジウム, 2007.02.
229. Kenji Kaneko, Keisuke Sato, Zenji Horita and Koji Inoke, Characterization of precipitates by three-dimensional electron tomography, The 6th Pacific Rim International Conference on Advanced Materials and Processing, 2007.11, Structures and morphologies of Ge precipitates in an Al-Ge alloy were characterized by a combination of transmission electron microscopy and three-dimensional electron tomography. Faceting of the precipitates was clearly seen using transmission electron microscopy and varieties of precipitate morphologies were identified by three-dimensional electron tomography..
230. Ayumu Umemoto, Koichi Hayashi, Kyoko Hayano, Noritaka Saito, Kenji Kaneko, Kunihiko Nakashima, Effect of mo powder surface condition on fabrication of Mo-SiO2 functionally graded materials with slipcasting method, 2nd International Conference on Characterization and Control of Interfaces for High Quality Advanced Materials, and Joining Technology for New Metallic Glasses and Inorganic Materials, The conventional high intensity discharge lamps are made of Mo foil-sealing method, in which the Mo-metal of 30 μm thick is sandwiched by the fused silica envelope. The conventional high intensity discharge lamps therefore requires cooling system to reduce the thermal stress between Mo and fused silica during the switching operation and a long sealing zone is usually required to complete hermeticity, especially in high power devices, so that the production of compact high intensity discharge lamps has been a Herculean task. We show the invention of the new type of hermetically-sealed high intensity discharge lamps, made of Mo-SiO2 functionally graded material (FGM) as an electrode and a sealing component. In the case of high intensity discharge lamps with Mo-SiO2 FGM (FGM-Lamp), the thermal expansion coefficient between Mo and SiO2 is functionally graded so that it tolerates a large numbers of heating cycles, with no cooling system are required. Furthermore lamps survive without breakage. The W electrode is totally separated from the lamp envelope by the FGM, so that no leakage of the luminous elements or gases takes place, when a large gas pressure exists inside a lamp. In this paper, effects of Mo powder surface conditions on the fabrication of Mo-SiO 2 FGM have been investigated. Mo-SiO2 FGM with as-received Mo powder revealed that the Mo particles were homogenously distributed, which resulted in no microscopic compositional gradient. In contrast. Mo-SiO 2 FGM with pre-treated Mo powder provided a uniform gradient from the conductive part (Mo-rich phase) to the sealing part (amorphous silica)..
231. 金子賢治, 3次元電子線トモグラフィによる材料解析, 東北大学多元研講演会, 2006.11.
232. Yoichi Takeda, Naohiko Shimada, Kenji Kaneko, Kazuo Sakurai, Seiji Shinkai, Property of polysaccharide nano gel involves polyion complex consists of cationic polymer/ DNA, 55th SPSJ Annual Meeting, 2006.10, It is known to be hydrophobic as for the Polyion complex that consisits of DNA and the cation when it is equal compared with the cation/anion. On the other hand, when the DMSO solution of β glucan is dropped to water, the Nano gel that has the hydrophobic area internally is formed. We found that DNA and the cation complex be able to be involved in the Nano gel of Schizophyllan that one of β glucan for the first time in this research. Moreover, the application of CpG DNA delivery will be described..
233. K. Inoke, K. Kaneko, M. Weyland, P. A. Midgley amd Z. Horita, Severe local strain & the plastic deformation of Guinier-Preston zones in the Al-Ag system revealed by 3D electron tomography, The 16th International Microscopy Congress, 2006.09, [URL].
234. 池田篤志, 伊藤小百合, 菊池純一, 金子賢治, 沼田宗典, 櫻井和朗, 新海征治, 生体高分子によるC60の水溶化, 第55回高分子学会年次大会, 2006.05.
235. 伊藤小百合, 池田篤志, 菊池純一, 金子賢治, 沼田宗典, 櫻井和朗, 新海征治, 生体高分子を可溶化剤とするC60の新規水溶化, 日本化学会第86回春季年会, 2006.03.
236. 沼田宗典・原口修一・金子賢治・櫻井和朗・新海征治, 多糖・シゾフィランのラッピング特性を利用した新規ブロックポリマーの創製, 日本化学会第86回春季年会, 2006.03.
237. 藤越千明・久保羊平・竹内正之・新海征治・金子賢治, カーボンナノチューブの配列制御 (5), 日本化学会第86回春季年会, 2006.03.
238. 藤越千明・久保羊平・竹内正之・新海征治・金子賢治, 一次元高分子の配列制御 (4), 日本化学会第86回春季年会, 2006.03.
239. 竹林新二・久保羊平・金子賢治・竹内正之・新海征治, 共役系高分子の配列制御 (3), 日本化学会第86回春季年会, 2006.03.
240. 若林里衣・久保羊平・金子賢治・竹内正之・新海征治, 共役系高分子の配列制御 (1), 日本化学会第86回春季年会, 2006.03.
241. Yoshiyasu Kawasaki, Koji Neishi, Yuichi Miyahara, Katsuaki Nakamura, Kenji Kaneko, Michihiko Nakagaki, Zenji Horita, Application of severe torsion straining process for grain refinement of steel, 3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3, Severe torsion straining process (STSP) is a useful technique for grain refinement of metallic materials. With this process, a local heated zone is produced in a rod and one side of the rod is rotated with respect to the other so that torsion strain is introduced into the local heated zone. Severe straining is then achieved continuously throughout the rod by simultaneous rotation and longitudinal movement of the rod. Thus, the STSP is a continuous process and a die-less process for grain refinement. It is suggested that the STSP provide potential for commercialization. In this study, S45C steel rods with 12 mm in diameter were subjected to STSP. This process was conducted at a temperature of 923 K (650°C) with various ratios of rotation to longitudinal movement of a rod. Local heating was made using an induction coil and both sides of the local heated zone were cooled by water spray. Microscopy observation revealed that the initial grain size of ∼15 μm was reduced to ∼2 μm using the STSP..
242. Katsuaki Nakamura, Koji Neishi, Kenji Kaneko, Michihiko Nakagaki, Zenji Horita, Continuous grain refinement using severe torsion straining process, 3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3, This study presents a new rapid continuous process for grain refinement in metallic materials through severe plastic deformation (SPD). The new process, designated in this study the severe torsion straining process (STSP), is applicable to a wide range of alloys based on aluminum, magnesium and copper including carbon steel. This process consists of producing a local heated zone in a rod and cooling both sides of the heated zone by spray water while rotating one end with the other. Thus, torsion strain is introduced in the local heated zone. The STSP can be continuous because the straining is achieved while the rod is shifted along the longitudinal axis of die rod. Furthermore, the process requires no die, suggesting a potential for commercialization of grain refinement through SPD. In this study, STSP was applied to an Al-Mg alloy and a Mg-Al-Zn alloy. It is shown that STSP is effective for both alloys so that the grain size is reduced to ∼1.5 μm for the Al alloy and ∼0.9 μm for the Mg alloy. Tensile testing showed that the strength is increased with a minimal decrease in uniform elongation. There is a critical ratio between rotation speed and moving speed, which defines the feasibility of STSP operation without breaking the rod. The grain size tends to be lowered as the ratio is close to the critical value..
243. Munenori Numata, Shunichi Haraguchi, Tomohisa Fujisawa, Kenji Kaneko, Kazuo Sakurai, Seiji Shinkai, Creation of novel nanomaterials utilizing biomaterials based on natural polysaccharide-conjugated polymer complex, 55th SPSJ Annual Meeting, It is already known that β-1,3-glucans form a hydrophobic cavity within the helical superstructure, which is surrounded by hydrophilic side-glucoses or primary OH groups. This unique core-shell structure resembles that of cyclodextrins, which are well-established hosts for C60. Therefore, the fact encouraged us to pursue the possibility that β-1,3-glucans could act as a novel one-dimensional host for single-walled carbon nanotubes (SWNTs). As expected, β-1,3-glucans can interact with SWNTs to produce unique nanocomposites, in which SWNTs are entrapped within a one-dimensional hollow constructed by the helical superstructure of β-1,3-glucans. Moreover, various conductive polymers are also entrapped within the one-dimensional hollow to be arranged into the one-dimensional array. Since the surface is covered with β-1,3-glucans, the complex has potential to be bionanomaterials, where β-1,3-glucans act as an interface between the conjugated polymer and biologically important molecules. We tested this idea utilizing schizophyllan/conjugated polymer complex..
244. Koji Neishi, Akihiko Higashino, Yuichi Miyahara, Katsuaki Nakamura, Kenji Kaneko, Michihiko Nakagaki, Zenji Horita, Grain refinement of commercial Al-Mg alloy using severe torsion straining process, 3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3, Severe plastic deformation (SPD) makes it possible to refine grain size in many metallic materials. Recently, we have developed a new SPD process designated the severe torsion straining process (STSP). This process requires no die but one side of a rod is rotated with respect to the other while producing a local heated zone in the rod and cooling both sides of the heated zone. Torsion strain is then introduced in the local heated zone. The STSP can be a continuous process because the rod is moved in the longitudinal direction while introducing torsion strain through the rotation. For grain refinement using the STSP, various factors may affect, which are the rotation speed, moving speed, straining temperature, cooling rate and diameter of the rod. In this study, the STSP is applied to grain refinement of an A5056 Al-Mg commercial alloy and the factors affecting the grain refinement are optimized. STSP was conducted at a temperature in the range from 573K to 723K. Microstracture was observed by optical microscopy, scanning electron microscopy with an orientation imaging system, and transmission electron microscopy. Microscopy observations revealed that the grain size was reduced to ∼0.9 um, when STSP was conducted at 573K with a rotation speed of 10 rpm and moving speed of 50 mm/min. There is a critical ratio of rotation speed to moving speed above which the rod breaks. The grain size tends to be finer as the straining temperature is lower, the cooling rate is faster and the ratio of rotation speed to moving speed is closer to the critical value..
245. Y. Hayashi, T. Tokunaga, Kenji Kaneko, S. J. Henley, V. Stolojan, J. D. Carey, S. R P Silva, Microstructure analyses of metal-filled carbon nanotubes synthesized by microwave plasma-enhanced chemical vapour deposition, 2006 IEEE Conference on Emerging Technologies - Nanoelectronics, Pd/Co-based metal-filled carbon nanotubes (MF-CNTs) were synthesized by a microwave plasma-enhanced chemical vapour deposition method using a bias-enhanced growth technique. Pd/Co-based MF-CNTs were analyzed by scanning electron microscopy (SEM), transmission electron microscopy (TEM) electron energy loss spectroscopy (EELS), and Raman spectroscopy. MF-CNTs were well-aligned and uniform in size on a Si substrate. Both multiwall nanotube carbon nanotubes (CNTs) and herringbone (or stacked cups structure) structures were observed. High-resolution TEM revealed that MF-CNTs were composed of highly ordered graphite layers, and the elemental maps of EELS indicate that both Co and Pd metals are present inside the nanotubes. TEM results clearly showed that both Pd and Co metals were successfully encapsulated into the CNTs.. We observed a low value for the Raman intensity ratio between D (1355 cm-1) and G (1590 cm-1) bands with no shift of the G-peak position and no broadening of the G-peak, indicative of high quality Pd/Co-based MF-CNTs. Based on TEM characterization, we propose a description for the encapsulating mechanisms..
246. Yuichi Miyahara, Naoki Emi, Koji Neishi, Katsuaki Nakamura, Kenji Kaneko, Michihiko Nakagaki, Zenji Horita, Microstructures and mechanical properties of Mg alloy after severe torsion straining process, 3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3, Grain refinement is attempted using severe plastic deformation (SPD) through the severe torsion straining process (STSP) which we have developed recently. The STSP is a continuous process for grain refinement without requirement of any die. In this study, an AZ61 Mg alloy was subjected to STSP at a temperature of 573 K with a rotation speed of 10 rpm and a moving speed of 200 mm/min. With this process, an initial grain size of ∼20 μm was reduced to ∼2∼3 μm. Room temperature compression tests revealed that there were no cracks after 15% of compression for the STSP sample whereas fracture occurred for a conventionally extruded sample. For compression tests at 473 K, no cracks occurred in the STSP samples after 80% compression but compression was feasible without cracking only up to 20% for an extruded sample. It is shown that the STSP can be useful for grain refinement and ductility improvement of the AZ61 Mg alloy..
247. Ayumu Umemoto, Koichi Hayashi, Kunihiko Nakashima, Noritaka Saito, Kenji Kaneko, Keisaku Ogi, Mo-SiO2 functionally graded materials for high intensity discharge lamp, 6th Pacific Rim Conference on Ceramic and Glass Technology, PacRim6, The conventional high intensity discharge lamps are made of Mo foil-sealing method, in which the Mo-metal of 30 μm thick is sandwiched by the fused silica envelope. The conventional high intensity discharge lamps therefore requires cooling system to reduce the thermal stress between Mo and fused silica during the switching operation and a lung sealing zone is usually required to complete hermeticity, especially in high power devices, so that the production of compact high intensity discharge lamps has been a Herculean task, Here, we show the invention of the new type of hermetically-sealed high intensity discharge lamps, made of Mo-SiO2 functionally graded material (FGM) as an electrode and a sealing component. In the case of high intensity discharge lamps with Mo-SiO2 FGM (FGM-Lanip), the thermal expansion coefficient between Mo and SiO2 is functionally graded so that it tolerates a large number of heating cycles, with no cooling system are required, Furthermore lamps survive without breakage of lamp takes place, The W electrode is totally separated from the lamp envelope by the FGM, so that no leakage of the luminous elements or gases takes place, when a large gas pressure exists inside a lamp..
248. Takahiro Kaseyamaj, Yohei Kubo, Kenji Kaneko, Masayuki Takeuchi, Seiji Shinkai, Nanoscale alignment of conjugated polymers by supramolecular approach(2), 55th Society of Polymer Science Japan Symposium on Macromolecules, We designed and synthesized a compound 1 that can align conjugated polymers. This compound has palladium complexes as molecular recognition units and can align polyanilines. The morphologies of the supramolecular assemblies consisting of this compound and polyaniline were monitored by UV-vis spectroscopy and TEM..
249. Shinji Takebsyashi, Yohei Kubo, Kenji Kaneko, Masayuki Takeuchi, Seiji Shinkai, Nanoscale alignment of conjugated polymers by a supramolecular approach, 55th Society of Polymer Science Japan Symposium on Macromolecules, Exploring new methods for alignment of conjugated polymers is of importance for the production of materials having optimized properties. In these days, several methods for alignment of conjugated polymers have been reported by many research groups. We have recently proposed a new concept for alignment of conjugated polymers where the porphyrinatozinc tetramer was designed and utilized as an Aligner; the molecule binds amino functionalized cojugated polymers (CP1) to align them into the two-dimensional super structures. We here report an attempt on three-dimensional alignment of conjugated polymers by a poly-Aligner..
250. L. Miao, T. Jiang, S. Tanemura, M. Tanemura, M. Mori, S. Toh, Kenji Kaneko, Photochromic Ag-TiO2 thin films fabricated by dual-target helicon magnetron sputtering, AICAM 2005 - Asian International Conference on Advanced Materials, Photochromic material Ag-TiO2 thin films are fabricated on quartz substrate by dual -target helicon magnetron sputtering. The phototchromic behavior is investigated for the sample loaded with 90% Ag. Spheres, ellipsoids and polyhedra shape of Ag particles with wide range size (5∼100 nm) are dispersed in the TiO2 amorphous matrix observed by transmission electron microscopy. The spectral hole burned by the irradiation of laser at the wavelength 532 nm can be explained by a particle-plasmon-assisted electron transfer from Ag nanoparticles to TiO2 and subsequent trapping by adsorbed molecular oxygen. Moreover, the mechanism of the slow recovery after photochromism is suggested as a slow thermal release of electrons from oxygen trapping centers and subsequent capture into the Ag nanoparticles..
251. Masayuki Takeuchi, Chiaki Fujikoshi, Yohei Kubo, Kenji Kaneko, Seiji Shinkai, Sequential organization by a supramolecular twining approach toward the alignment of conjugated polymers, 55th SPSJ Annual Meeting, Here we report that porphyrin polymers (Twining polymer; Twimer) possessing conjugated polymer binding sites would twine around, and align them in a noncovalent fashion (Fig.1). The morphologies of the resulting supramolecular assemblies between twimers and conjugated polymers were monitored by UV-Vis, fluorescence spectroscopies, CLSM, PM, and HRTEM. Very interestingly, they afforded novel well-regulated structures..
252. Atsushi Ikeda, Sayuri Ito, Jun Ichi Kikuchi, Kenji Kaneko, Munenori Numata, Kazuo Sakurai, Seiji Shinkai, Solubilization of C 60 by using biopolymers, 55th SPSJ Annual Meeting, The ready availability of [60]fullerene (C 60) has increasingly invited exploration of their outstanding new physical and chemical properties. Water-solubilization of C 60 holds potential in the application for various medicinal uses. The use of biomolecules as solubilizing agents of C 60 is preferable in order to be applied for medicinal fields because of little or less toxicity. Taking into account these aims, we have now chosen various polysaccharides as solubilizing agents such as amylose and schizophyllan (SPG). We have discovered that amylose and SPG can solved C 60 in water and form the one dimensional ordered C 60 in the hydrophobic cavities..
253. Masayuki Takeuchi, Osamu Hirata, Tomohiro Ikeda, Masayuki Shibata, Kenji Kaneko, Seiji Shinkai, Supramolecular systems utilizing rotational units, 55th Society of Polymer Science Japan Symposium on Macromolecules, We designed portphyrin 1 bearing rotational units at meso-position and porphyrin polymer Pn which has double decker Ce(IV) bisporphyrinate as rotational units and Zn(II) porphyrin as recognition sites alternately. We expected that compound 1 could form one-dimensional supramolecular polymer with Pd complexes, whereas polymer Pn would be expected to fold at the vertex double-decker porphyrin complex in the presence of guests..
254. Koji Inoke, Kenji Kaneko, Zenji Horita, Three-dimensional imaging of shear band produced by ECAP process in Al-Ag alloy, 3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3, A significant change in microstracture occurs during the application of severe plastic deformation (SPD) such as by equal-channel angular pressing (ECAP). In this study, intense plastic strain was imposed on an Al-10.8wt%Ag alloy by the ECAP process. The amount of strain was controlled by the numbers of passes. After 1 pass of ECAP, shear bands became visible within the matrix. With increasing numbers of ECAP passes, the fraction of shear bands was increased. In this study, the change in microstructures was examined by three-dimensional electron tomography (3D-ET) in transmission electron microscopy (TEM) or scanning transmission electron microscopy (STEM). With this 3D-ET method, it was possible to conduct a precise analysis of the sizes, widths and distributions of the shear bands produced by the ECAP process. It is demonstrated that the 3D-ET method is promising to understand mechanisms of microstractural refinement using the ECAP process..
255. 竹内正之・田中智史・金子賢治・新海征治, ポルフィリンを基体とした超分子集合体の形態制御, 第54回高分子討論会, 2005.09.
256. 白川三千紘・藤田典史・谷 崇博・金子賢治・新海征治, 8-キノリノール白金(II)錯体を基体とした燐光性低分子ゲルの発光特性, 第55回錯体化学討論会, 2005.09.
257. 沼田宗典, 金子賢治, 櫻井和郎, 新海征治, 多糖・β1,3 グルカンを1次元ホストとした新規ナノコンポジットの創製, 第20 回 生体機能関連化学シンポジウム, 2005.09.
258. 佐藤和好, 阿部浩也, 内藤牧男, 金子賢治, 機械的手法によるLaMnO3 ナノ粒子の合成とその反応過程の解析, 日本セラミックス協会 第18回秋季シンポジウム, 2005.09.
259. Kenji KANEKO, Ultrananoscopic characterization of nano-powders and particles by transmission electron microscopes, The 6th Pacific Rim Conference on Ceramics and Glass Technology, 2005.09.
260. 久保羊平・若林里衣・藤越千明・金子賢治・竹内正之・新海征治, 分子を用いた共役高分子の配列制御[I], 第54回高分子討論会, 2005.05.
261. 田中智史・金子賢治・竹内正之・新海征治, キラルゲストにより誘起されたポルフィリン有機ゲルのらせん状超分子集合体, 日本化学会第85回春季年会, 2005.03.
262. 田中智史・白川三千紘・金子賢治・竹内正之・新海征治, ピリジン-カルボン酸相互作用により制御されたポルフィリン有機ゲルの超分子集合体, 日本化学会第85回春季年会, 2005.03.
263. 久保羊平・若林里衣・竹内正之・新海征治・金子賢治, 超分子を用いた共役高分子の配列制御(1), 日本化学会第85回春季年会, 2005.03.
264. Chiaki Fujikoshi, Yohei Kubo, Masayuki Takeuchi, Seiji Shinkai, Kenji Kaneko, Alignment of conjugated polymers by supramolecular porphyrin polymer (3), 54th SPSJ Symposium on Macromolecules, Here we report that porphyrin polymer (Twining polymer; Twimer) possessing conjugated polymer binding sites would twine around, and align them in a noncovalent fashion (Fig.1). The morphologies of the resulting supramolecular assemblies between twimers and conjugated polymers were monitored by UV-Visible, fluorescence spectroscopies, CLSM, PM, and HR TEM. Very interestingly, they afforded novel well-regulated network structure..
265. Yohei Kubo, Rie Wakabayashi, Chiaki Fujikoshi, Kenji Kaneko, Masayuki Takeuchi, Seiji Shinkai, Alignment of conjugated polymers by supramolecular porphyrin oligomer (1), 54th SPSJ Symposium on Macromolecules, We here report a preliminary step toward alignment and organization of conjugated polymers by an Aligner molecule with an allosteric function. Aligner molecules 1 and 2, which show positive homotropic allosterism, can bind a guest poly(phenylene-ethynylene) bearing bis(methylaminomethyl)benzene moieties (P1) in their porphinatozinc clefts to organize assemblies of P1. The binding studies were conducted by UV-Vis, fluorescent spectroscopy, AFM and TEM..
266. Rie Wakabayashi, Yohei Kubo, Masayuki Takeuchi, Seiji Shinkai, Kenji Kaneko, Alignment of conjugated polymers by supramolecular porphyrin oligomer (2), 54th SPSJ Symposium on Macromolecules, We proposed a novel approach for aligning and organizing of conjugated polymers by Aligners, which possess several binding sites for conjugated polymers. In this system, however, the supramolecular assemblies between Aligners and polymers are under thermodynamic control and could be destroyed by dilution or other external factors. Aligner 3, which possesses olefins as reaction sites, can bind a guest poly(phenylene-ethynylene) (poly-PPE) and organize assemblies of poly-PPEs. These assemblies were able to be immobilized by metathesis reaction..
267. Masayuki Takeuchi, Satoshi Tanaka, Kenji Kaneko, Seiji Shinkai, Porphyrin-based supramoleculr assmenbies, 54th SPSJ Symposium on Macromolecules, Here we report that the morphology of one-dimensional aggregates composed of porphyrins can be controlled by the peripheral hydrogen-bond donating/accepting groups and van der Waals interactions among alkyl chains introduced in the orthogonal axis toward the porphyrin-porphyrin π π stacking axis. The supramolecular assemblies of porphyrin derivatives were monitored by UV-Visible, XRD, SEM, TEM, and HR-TEM. Very interestingly, they afforded a variety of supramolecular morphologies such as helical ribbon, sphere, doughnut, and cylinder depending on the environmental conditions..
268. 沼田宗典, 長谷川輝明, 金子賢治, 櫻井和郎, 新海征治, β1,3 グルカンを一次元ホストとして利用した機能性材料の創製, 第19 回 生体機能関連化学シンポジウム, 2004.10.

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